2,2-dimethyl-propionic acid 4-benzyl-1-hydroxy-6-methyl-1,3-dihydro-furo[3,4-c]pyridin-7-yl ester

Base Information

Chemical Name:2,2-dimethyl-propionic acid 4-benzyl-1-hydroxy-6-methyl-1,3-dihydro-furo[3,4-c]pyridin-7-yl ester
CAS No.:860462-16-4
Molecular Formula:C₂₀H₂₃NO₄
Molecular Weight:341.407
Hs Code.:

2,2-dimethyl-propionic acid 4-benzyl-1-hydroxy-6-methyl-1,3-dihydro-furo[3,4-<i>c</i>]pyridin-7-yl ester

Synonyms:2,2-dimethyl-propionic acid 4-benzyl-1-hydroxy-6-methyl-1,3-dihydro-furo[3,4-c]pyridin-7-yl ester

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Chemical Property of 2,2-dimethyl-propionic acid 4-benzyl-1-hydroxy-6-methyl-1,3-dihydro-furo[3,4-c]pyridin-7-yl ester

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Technology Process of 2,2-dimethyl-propionic acid 4-benzyl-1-hydroxy-6-methyl-1,3-dihydro-furo[3,4-c]pyridin-7-yl ester

There total 1 articles about 2,2-dimethyl-propionic acid 4-benzyl-1-hydroxy-6-methyl-1,3-dihydro-furo[3,4-c]pyridin-7-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 258531-72-5
3-trimethylmethylcarbonyl-6-(benzyl)pyridoxal monomethyl acetal

: 860462-16-4
2,2-dimethyl-propionic acid 4-benzyl-1-hydroxy-6-methyl-1,3-dihydro-furo[3,4-c]pyridin-7-yl ester

Guidance literature:: With sulfuric acid; In water; acetone; at 48 ℃; for 48h;
DOI:10.1016/j.bcp.2005.04.021

Reference yield: 68.0%

: 860462-16-4
2,2-dimethyl-propionic acid 4-benzyl-1-hydroxy-6-methyl-1,3-dihydro-furo[3,4-c]pyridin-7-yl ester

: 67-56-1
methanol

: 860462-17-5
6-(benzyl)pyridoxal-4-dimethylacetal

Guidance literature:: With potassium hydroxide; for 0.166667h;
DOI:10.1016/j.bcp.2005.04.021

Reference yield:

: 860462-16-4
2,2-dimethyl-propionic acid 4-benzyl-1-hydroxy-6-methyl-1,3-dihydro-furo[3,4-c]pyridin-7-yl ester

: 883747-34-0
6-benzyl-5-chloromethyl-4-dimethoxymethyl-2-methyl-pyridin-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / KOH / 0.17 h

2: 100 percent / thionyl chloride / benzene / 0.08 h

With potassium hydroxide; thionyl chloride; In benzene; 1: ring cleavage; methylation / 2: chlorination;
DOI:10.1016/j.bcp.2005.04.021