methyl 2-{[(4-methoxyphenyl)methyl][methyl(phenyl)carbamoyl]amino}butanoate

Base Information

Chemical Name:methyl 2-{[(4-methoxyphenyl)methyl][methyl(phenyl)carbamoyl]amino}butanoate
CAS No.:1462367-24-3
Molecular Formula:C₂₁H₂₆N₂O₄
Molecular Weight:370.448
Hs Code.:

Synonyms:methyl 2-{[(4-methoxyphenyl)methyl][methyl(phenyl)carbamoyl]amino}butanoate

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Chemical Property of methyl 2-{[(4-methoxyphenyl)methyl][methyl(phenyl)carbamoyl]amino}butanoate

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Technology Process of methyl 2-{[(4-methoxyphenyl)methyl][methyl(phenyl)carbamoyl]amino}butanoate

There total 1 articles about methyl 2-{[(4-methoxyphenyl)methyl][methyl(phenyl)carbamoyl]amino}butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1462367-24-3
methyl 2-{[(4-methoxyphenyl)methyl][methyl(phenyl)carbamoyl]amino}butanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0.17 h / Inert atmosphere; Molecular sieve

1.2: 18 h / 20 °C / Inert atmosphere; Molecular sieve

1.3: 18 h / 20 °C / Inert atmosphere

2.1: triethylamine / 1,2-dimethoxyethane / 0.17 h / Inert atmosphere

2.2: 20 h / Inert atmosphere; Reflux

With triethylamine; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1039/c3cc46193a

Reference yield: 98.0%

: 1462367-24-3
methyl 2-{[(4-methoxyphenyl)methyl][methyl(phenyl)carbamoyl]amino}butanoate

: 1462367-26-5
2-{[(4-methoxyphenyl)methyl][methyl(phenyl)carbamoyl]amino}butanoic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; water; at 45 ℃; for 20h; Inert atmosphere;
DOI:10.1039/c3cc46193a

Reference yield:

: 1462367-24-3
methyl 2-{[(4-methoxyphenyl)methyl][methyl(phenyl)carbamoyl]amino}butanoate

: 50-12-4
mephenytoin

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide / water; tetrahydrofuran / 20 h / 45 °C / Inert atmosphere

2: lithium chloride; lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

3: ammonium cerium (IV) nitrate / water; acetonitrile / 1 h / 0 °C / Inert atmosphere

With ammonium cerium (IV) nitrate; lithium chloride; lithium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; water; acetonitrile;
DOI:10.1039/c3cc46193a