(2-chlorophenyl)<4-chloro-2-(3,3-dimethoxypropanyl)phenyl>methanone imine

Base Information

Chemical Name:(2-chlorophenyl)<4-chloro-2-(3,3-dimethoxypropanyl)phenyl>methanone imine
CAS No.:101713-35-3
Molecular Formula:C₁₈H₁₉Cl₂NO₂
Molecular Weight:352.26
Hs Code.:

Synonyms:(2-chlorophenyl)<4-chloro-2-(3,3-dimethoxypropanyl)phenyl>methanone imine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-chlorophenyl)<4-chloro-2-(3,3-dimethoxypropanyl)phenyl>methanone imine

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Technology Process of (2-chlorophenyl)<4-chloro-2-(3,3-dimethoxypropanyl)phenyl>methanone imine

There total 6 articles about (2-chlorophenyl)<4-chloro-2-(3,3-dimethoxypropanyl)phenyl>methanone imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 67-56-1
methanol

: 101713-37-5
8-chloro-1-(2-chlorophenyl)-4,5-dihydro-3H-2-benzazepin-3-ol acetate

: 101713-34-2
8-chloro-1-(2-chlorophenyl)-4,5-dihydro-3-methoxy-3H-2-benzazepine

: 101713-35-3
(2-chlorophenyl)<4-chloro-2-(3,3-dimethoxypropanyl)phenyl>methanone imine

Guidance literature:: With hydrogenchloride; for 4h; Ambient temperature;
DOI:10.1021/jo00362a007

Reference yield: 38.0%

: 101713-37-5
8-chloro-1-(2-chlorophenyl)-4,5-dihydro-3H-2-benzazepin-3-ol acetate

: 101713-34-2
8-chloro-1-(2-chlorophenyl)-4,5-dihydro-3-methoxy-3H-2-benzazepine

: 101713-35-3
(2-chlorophenyl)<4-chloro-2-(3,3-dimethoxypropanyl)phenyl>methanone imine

Guidance literature:: With hydrogenchloride; for 4h; Ambient temperature;
DOI:10.1021/jo00362a007

Reference yield:

: 76049-54-2
N-<<4-chloro-2-(2-chlorobenzoyl)phenyl>-3-propynyl>isoindole-1,3(2H)-dione

: 101713-35-3
(2-chlorophenyl)<4-chloro-2-(3,3-dimethoxypropanyl)phenyl>methanone imine

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / H₂ / Raney nickel / tetrahydrofuran / 760 Torr / Ambient temperature

2: 66 percent / 40percent aq. methylamine / ethanol / 6 h / Ambient temperature

3: 96 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 0.5 h

4: 77 percent / 4 h / Heating

5: 38 percent / HCl / 4 h / Ambient temperature

With hydrogenchloride; hydrogen; 3-chloro-benzenecarboperoxoic acid; methylamine; nickel; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jo00362a007