5-(2,4-difluorophenoxy)-6-nitroindan

Base Information

Chemical Name:5-(2,4-difluorophenoxy)-6-nitroindan
CAS No.:81614-72-4
Molecular Formula:C₁₅H₁₁F₂NO₃
Molecular Weight:291.254
Hs Code.:

Synonyms:5-(2,4-difluorophenoxy)-6-nitroindan

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Chemical Property of 5-(2,4-difluorophenoxy)-6-nitroindan

Chemical Property:

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Technology Process of 5-(2,4-difluorophenoxy)-6-nitroindan

There total 7 articles about 5-(2,4-difluorophenoxy)-6-nitroindan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 367-27-1
2,4-difluorophenol

: 75369-85-6
5-Brom-6-nitroindan

: 81614-72-4
5-(2,4-difluorophenoxy)-6-nitroindan

Guidance literature:: With potassium tert-butylate; copper(l) chloride; In tert-butyl alcohol; for 7h; Heating;

Reference yield:

: 367-27-1
2,4-difluorophenol

: 75369-85-6
5-Brom-6-nitroindan

: 865-47-4
potassium tert-butylate

: 81614-72-4
5-(2,4-difluorophenoxy)-6-nitroindan

Guidance literature:: With hydrogenchloride; copper(I) chloride; In tert-butyl alcohol;

Reference yield:

: 24425-40-9
indan-5-amine

: 81614-72-4
5-(2,4-difluorophenoxy)-6-nitroindan

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / cc H₂SO₄, HNO₃ / 1./ 0.5 h. 2./ 1 h. room temp.

2: 1./ cc H₂SO₄, NaNO₂, acetic acid, 2./ CuBr, NaBr, 16percent HBr / 1./ water, 1 h. 3-5 deg C_.

3: 38 percent / CuCl, potassium tert-butoxide / 2-methyl-propan-2-ol / 7 h / Heating

With sulfuric acid; potassium tert-butylate; hydrogen bromide; nitric acid; acetic acid; sodium bromide; copper(l) chloride; copper(I) bromide; sodium nitrite; In tert-butyl alcohol;