C₃₃H₃₂Cl₂N₂O₆S₂

Base Information

Chemical Name:C₃₃H₃₂Cl₂N₂O₆S₂
CAS No.:1207203-45-9
Molecular Formula:C₃₃H₃₂Cl₂N₂O₆S₂
Molecular Weight:687.665
Hs Code.:

C<sub>33</sub>H<sub>32</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₃₃H₃₂Cl₂N₂O₆S₂

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Chemical Property of C₃₃H₃₂Cl₂N₂O₆S₂

Chemical Property:

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Technology Process of C₃₃H₃₂Cl₂N₂O₆S₂

There total 13 articles about C₃₃H₃₂Cl₂N₂O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56243-25-5
1-benzyl-4-cyano-4-phenylpiperidine

: 1207203-45-9
C₃₃H₃₂Cl₂N₂O₆S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: water; sulfuric acid / 1 h / 100 °C

1.2: Cooling with ice

2.1: cyclohexa-1,3-diene / palladium 10% on activated carbon / methanol / 6 h / Reflux

3.1: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 3 h / 20 °C

4.1: boron tribromide / dichloromethane / 3 h / 20 °C / Cooling with ice

5.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 90 °C

6.1: triethylamine / dichloromethane / 1 h

With sulfuric acid; water; boron tribromide; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; cyclohexa-1,3-diene; triethylamine; palladium 10% on activated carbon; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1207202-89-8
1-({5-(2,4-Dichlorophenyl)-4-[4-(3-hydroxypropoxy)phenyl]thien-2-yl}carbonyl)-4-phenylpiperidine-4-carboxamide

: 124-63-0
methanesulfonyl chloride

: 1207203-45-9
C₃₃H₃₂Cl₂N₂O₆S₂

Guidance literature:: With triethylamine; In dichloromethane; for 1h;

Reference yield:

: 59084-07-0
1-benzyl-4-phenyl-piperidine-4-carboxylic acid amide; hydrochloride

: 1207203-45-9
C₃₃H₃₂Cl₂N₂O₆S₂

Guidance literature:: Multi-step reaction with 5 steps

1: cyclohexa-1,3-diene / palladium 10% on activated carbon / methanol / 6 h / Reflux

2: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 3 h / 20 °C

3: boron tribromide / dichloromethane / 3 h / 20 °C / Cooling with ice

4: potassium carbonate / N,N-dimethyl-formamide / 3 h / 90 °C

5: triethylamine / dichloromethane / 1 h

With boron tribromide; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; cyclohexa-1,3-diene; triethylamine; palladium 10% on activated carbon; In methanol; dichloromethane; N,N-dimethyl-formamide;