C₄₈H₅₇NO₅Si₂

Base Information

Chemical Name:C₄₈H₅₇NO₅Si₂
CAS No.:704906-68-3
Molecular Formula:C₄₈H₅₇NO₅Si₂
Molecular Weight:784.155
Hs Code.:

C<sub>48</sub>H<sub>57</sub>NO<sub>5</sub>Si<sub>2</sub>

Synonyms:C₄₈H₅₇NO₅Si₂

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Chemical Property of C₄₈H₅₇NO₅Si₂

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Technology Process of C₄₈H₅₇NO₅Si₂

There total 12 articles about C₄₈H₅₇NO₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 201230-82-2
carbon monoxide

: C₄₇H₅₈INO₄Si₂

: 704906-68-3
C₄₈H₅₇NO₅Si₂

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; triethylamine; In N,N-dimethyl acetamide; at 65 ℃; for 6h; under 760.051 Torr; Inert atmosphere;
DOI:10.1002/chem.201003489

Reference yield:

: C₁₆H₁₃NO₆

: 704906-68-3
C₄₈H₅₇NO₅Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: (-)-N-methylephedrine; zinc trifluoromethanesulfonate; triethylamine / toluene / 18.25 h / 20 °C / Inert atmosphere

2.1: 1H-imidazole / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1 h / -78 - 0 °C / Inert atmosphere

3.2: 5 h / -78 - 20 °C / Inert atmosphere

4.1: potassium carbonate / methanol / 1.5 h / 20 °C / Inert atmosphere

5.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C / Inert atmosphere

5.2: 1 h / 0 - 20 °C / Inert atmosphere

6.1: N-iodo-succinimide; silver nitrate / acetone / 2 h / 20 °C / Darkness; Inert atmosphere

7.1: pyridine; potassium diazodicarboxylate; acetic acid / methanol / 1 h / Inert atmosphere

8.1: methanol; ammonium chloride; zinc / tetrahydrofuran; water / 1 h / 20 °C / Sonication; Inert atmosphere

9.1: 1H-imidazole / dichloromethane / 10 h / 20 °C / Inert atmosphere

10.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl acetamide / 6 h / 65 °C / 760.05 Torr / Inert atmosphere

With pyridine; 1H-imidazole; methanol; bis-triphenylphosphine-palladium(II) chloride; N-iodo-succinimide; (-)-N-methylephedrine; potassium diazodicarboxylate; tetra-(n-butyl)ammonium iodide; zinc trifluoromethanesulfonate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; ammonium chloride; silver nitrate; acetic acid; triethylamine; zinc; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl acetamide; water; acetone; toluene; mineral oil;
DOI:10.1002/chem.201003489

Reference yield:

: C₃₁H₃₈INO₅Si

: 704906-68-3
C₄₈H₅₇NO₅Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; ammonium chloride; zinc / tetrahydrofuran; water / 1 h / 20 °C / Sonication; Inert atmosphere

2: 1H-imidazole / dichloromethane / 10 h / 20 °C / Inert atmosphere

3: bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl acetamide / 6 h / 65 °C / 760.05 Torr / Inert atmosphere

With 1H-imidazole; methanol; bis-triphenylphosphine-palladium(II) chloride; ammonium chloride; triethylamine; zinc; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; water;
DOI:10.1002/chem.201003489