(S)-methyl 3-(tert-butoxycarbonyl(4-(cyclopropyl(2,3-dichlorobenzyl)amino)-1-(methoxymethoxy)-4-oxobutan-2-yl)amino)propanoate

Base Information

Chemical Name:(S)-methyl 3-(tert-butoxycarbonyl(4-(cyclopropyl(2,3-dichlorobenzyl)amino)-1-(methoxymethoxy)-4-oxobutan-2-yl)amino)propanoate
CAS No.:1361293-53-9
Molecular Formula:C₂₅H₃₆Cl₂N₂O₇
Molecular Weight:547.476
Hs Code.:

Synonyms:(S)-methyl 3-(tert-butoxycarbonyl(4-(cyclopropyl(2,3-dichlorobenzyl)amino)-1-(methoxymethoxy)-4-oxobutan-2-yl)amino)propanoate

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Chemical Property of (S)-methyl 3-(tert-butoxycarbonyl(4-(cyclopropyl(2,3-dichlorobenzyl)amino)-1-(methoxymethoxy)-4-oxobutan-2-yl)amino)propanoate

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Technology Process of (S)-methyl 3-(tert-butoxycarbonyl(4-(cyclopropyl(2,3-dichlorobenzyl)amino)-1-(methoxymethoxy)-4-oxobutan-2-yl)amino)propanoate

There total 4 articles about (S)-methyl 3-(tert-butoxycarbonyl(4-(cyclopropyl(2,3-dichlorobenzyl)amino)-1-(methoxymethoxy)-4-oxobutan-2-yl)amino)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1361293-52-8
(S)-methyl 3-(tert-butoxycarbonyl(4-(cyclopropyl(2,3-dichlorobenzyl)amino)-1-hydroxy-4-oxobutan-2-yl)amino)propanoate

: 107-30-2
chloromethyl methyl ether

: 1361293-53-9
(S)-methyl 3-(tert-butoxycarbonyl(4-(cyclopropyl(2,3-dichlorobenzyl)amino)-1-(methoxymethoxy)-4-oxobutan-2-yl)amino)propanoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; sodium iodide; In 1,2-dimethoxyethane; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 1361293-50-6
(S)-3-Amino-N-cyclopropyl-N-(2,3-dichlorobenzyl)-4-hydroxybutanamide

: 1361293-53-9
(S)-methyl 3-(tert-butoxycarbonyl(4-(cyclopropyl(2,3-dichlorobenzyl)amino)-1-(methoxymethoxy)-4-oxobutan-2-yl)amino)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 50 °C / Inert atmosphere

2: sodium hydrogencarbonate / 1,4-dioxane / 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dimethoxyethane / 0 - 20 °C / Inert atmosphere

With sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; sodium iodide; In 1,4-dioxane; methanol; 1,2-dimethoxyethane;

Reference yield:

: 1361293-49-3
(S)-benzyl 4-(cyclopropyl(2,3-dichlorobenzyl)amino)-1-hydroxy-4-oxobutan-2-ylcarbamate

: 1361293-53-9
(S)-methyl 3-(tert-butoxycarbonyl(4-(cyclopropyl(2,3-dichlorobenzyl)amino)-1-(methoxymethoxy)-4-oxobutan-2-yl)amino)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1: trimethylsilyl iodide / acetonitrile / 0.25 h / 20 °C / Inert atmosphere

2: methanol / 50 °C / Inert atmosphere

3: sodium hydrogencarbonate / 1,4-dioxane / 20 °C / Inert atmosphere

4: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dimethoxyethane / 0 - 20 °C / Inert atmosphere

With trimethylsilyl iodide; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; sodium iodide; In 1,4-dioxane; methanol; 1,2-dimethoxyethane; acetonitrile;