9-triptycyltrimethyltin

Base Information

• Chemical Name: 9-triptycyltrimethyltin
• CAS No.: 59239-91-7
• Molecular Formula: C₂₃H₂₂Sn
• Molecular Weight: 417.138

Synonyms:9-triptycyltrimethyltin

Chemical Property of 9-triptycyltrimethyltin

Chemical Property:

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Technology Process of 9-triptycyltrimethyltin

There total 3 articles about 9-triptycyltrimethyltin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(trimethylstannyl)lithium (17946-71-3) + 9-bromotriptycene (15364-55-3) → triptycene (477-75-8) + 9-triptycyltrimethyltin (59239-91-7)

Guidance literature:

In tetrahydrofuran; at 0 ℃; Further Variations:; Reagents; Product distribution;

DOI:10.1021/jo001638w

Reference yield:

(trimethylstannyl)lithium (17946-71-3) + 9-bromo-10-chlorotriptycene (116263-71-9) → 9-chlorotriptycene (793-40-8) + 9-triptycyltrimethyltin (59239-91-7) + C20H12ClSn(CH3)3 + C20H12Sn(CH3)3Sn(CH3)3

Guidance literature:

In tetrahydrofuran; at 0 ℃; Further Variations:; Reagents; Product distribution;

DOI:10.1021/jo001638w

Reference yield:

(trimethylstannyl)lithium (17946-71-3) + 9,10-dibromotriptycene (795-42-6) → 9-bromotriptycene (15364-55-3) + 9-triptycyltrimethyltin (59239-91-7) + C20H12Sn(CH3)3Br + C20H12Sn(CH3)3Sn(CH3)3

Guidance literature:

In tetrahydrofuran; at 0 ℃; Further Variations:; Reagents; Product distribution;

DOI:10.1021/jo001638w

upstream raw materials:

(trimethylstannyl)lithium

9,10-dibromotriptycene

9-bromotriptycene

9-bromo-10-chlorotriptycene

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