(-)-2-{(1R)-1-[((1Z)-3-phenyl-1-propenyl)oxy]ethyl}-1,3,5-triisopropylbenzene

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Chemical Name:(-)-2-{(1R)-1-[((1Z)-3-phenyl-1-propenyl)oxy]ethyl}-1,3,5-triisopropylbenzene
CAS No.:210964-87-7
Molecular Formula:C₂₆H₃₆O
Molecular Weight:364.571
Hs Code.:

Synonyms:(-)-2-{(1R)-1-[((1Z)-3-phenyl-1-propenyl)oxy]ethyl}-1,3,5-triisopropylbenzene

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Chemical Property of (-)-2-{(1R)-1-[((1Z)-3-phenyl-1-propenyl)oxy]ethyl}-1,3,5-triisopropylbenzene

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Technology Process of (-)-2-{(1R)-1-[((1Z)-3-phenyl-1-propenyl)oxy]ethyl}-1,3,5-triisopropylbenzene

There total 3 articles about (-)-2-{(1R)-1-[((1Z)-3-phenyl-1-propenyl)oxy]ethyl}-1,3,5-triisopropylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 210964-92-4
2-{(1R)-1-[(3-phenyl-1-propynyl)oxy]ethyl}-1,3,5-triisopropylbenzene

: 210964-87-7
(-)-2-{(1R)-1-[((1Z)-3-phenyl-1-propenyl)oxy]ethyl}-1,3,5-triisopropylbenzene

Guidance literature:: With hydrogen; palladium on barium sulfate; In pyridine; for 5h; Yield given;
DOI:10.1021/jo9801162

Reference yield:

: 100-39-0
benzyl bromide

: 210964-87-7
(-)-2-{(1R)-1-[((1Z)-3-phenyl-1-propenyl)oxy]ethyl}-1,3,5-triisopropylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) KH, 3.) n-BuLi / 1) THF; 2) THF, -50 deg C, 15 min, -50 --> 20 deg C, 1 h; 3) THF, hexane, -70 deg C, 30 min, -70 to -40 deg C, 30 min; 4) THF, hexane, hexamethylphosphoramide, 20 deg C, 2 h

2: H₂ / Pd-BaSO₄ / pyridine / 5 h

With n-butyllithium; hydrogen; potassium hydride; palladium on barium sulfate; In pyridine;
DOI:10.1021/jo9801162

Reference yield:

: 181531-14-6
(R)-(+)-1-(2,4,6-triisopropylphenyl)ethanol

: 210964-87-7
(-)-2-{(1R)-1-[((1Z)-3-phenyl-1-propenyl)oxy]ethyl}-1,3,5-triisopropylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) KH, 3.) n-BuLi / 1) THF; 2) THF, -50 deg C, 15 min, -50 --> 20 deg C, 1 h; 3) THF, hexane, -70 deg C, 30 min, -70 to -40 deg C, 30 min; 4) THF, hexane, hexamethylphosphoramide, 20 deg C, 2 h

2: H₂ / Pd-BaSO₄ / pyridine / 5 h

With n-butyllithium; hydrogen; potassium hydride; palladium on barium sulfate; In pyridine;
DOI:10.1021/jo9801162