3a,6a-bis-(4-decyloxy-phenyl)-1,6-bis-(4-methoxy-benzyl)-tetrahydro-imidazo[4,5-d]imidazole-2,5-dione

Base Information

Chemical Name:3a,6a-bis-(4-decyloxy-phenyl)-1,6-bis-(4-methoxy-benzyl)-tetrahydro-imidazo[4,5-d]imidazole-2,5-dione
CAS No.:385818-27-9
Molecular Formula:C₅₂H₇₀N₄O₆
Molecular Weight:847.151
Hs Code.:

3a,6a-bis-(4-decyloxy-phenyl)-1,6-bis-(4-methoxy-benzyl)-tetrahydro-imidazo[4,5-<i>d</i>]imidazole-2,5-dione

Synonyms:3a,6a-bis-(4-decyloxy-phenyl)-1,6-bis-(4-methoxy-benzyl)-tetrahydro-imidazo[4,5-d]imidazole-2,5-dione

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Chemical Property of 3a,6a-bis-(4-decyloxy-phenyl)-1,6-bis-(4-methoxy-benzyl)-tetrahydro-imidazo[4,5-d]imidazole-2,5-dione

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Technology Process of 3a,6a-bis-(4-decyloxy-phenyl)-1,6-bis-(4-methoxy-benzyl)-tetrahydro-imidazo[4,5-d]imidazole-2,5-dione

There total 1 articles about 3a,6a-bis-(4-decyloxy-phenyl)-1,6-bis-(4-methoxy-benzyl)-tetrahydro-imidazo[4,5-d]imidazole-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 54582-35-3
p-methoxybenzylurea

: 156733-59-4
1,2-bis(4-(decyloxy)phenyl)ethane-1,2-dione

: 385818-27-9
3a,6a-bis-(4-decyloxy-phenyl)-1,6-bis-(4-methoxy-benzyl)-tetrahydro-imidazo[4,5-d]imidazole-2,5-dione

Guidance literature:: With trifluoroacetic acid; In benzene; for 24h; Heating;
DOI:10.1021/ja011651d

Reference yield: 28.0%

: 22262-60-8
methyl 3-bromo-2-(bromomethyl)propionate

: 385818-27-9
3a,6a-bis-(4-decyloxy-phenyl)-1,6-bis-(4-methoxy-benzyl)-tetrahydro-imidazo[4,5-d]imidazole-2,5-dione

: 2a,7b-bis-(4-decyloxy-phenyl)-2,3-bis-(4-methoxy-benzyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid methyl ester

Guidance literature:: With CsCO₃; In acetonitrile; for 20h; Heating;
DOI:10.1021/ja011651d

Reference yield:

: 385818-27-9
3a,6a-bis-(4-decyloxy-phenyl)-1,6-bis-(4-methoxy-benzyl)-tetrahydro-imidazo[4,5-d]imidazole-2,5-dione

: 2a,7b-bis-(4-decyloxy-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / CsCO₃ / acetonitrile / 20 h / Heating

2: 44 percent / ammonium cerium (IV) nitrate / acetonitrile; tetrahydrofuran; H₂O / 24 h / 20 °C

With ammonium cerium(IV) nitrate; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/ja011651d