C₂₉H₃₇NO₅

Base Information Edit

Chemical Name:C₂₉H₃₇NO₅
CAS No.:1394050-67-9
Molecular Formula:C₂₉H₃₇NO₅
Molecular Weight:479.616
Hs Code.:
Mol file:1394050-67-9.mol

C<sub>29</sub>H<sub>37</sub>NO<sub>5</sub>

Synonyms:C₂₉H₃₇NO₅

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Chemical Property of C₂₉H₃₇NO₅ Edit

Chemical Property:

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Technology Process of C₂₉H₃₇NO₅

There total 9 articles about C₂₉H₃₇NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1394050-29-3
C₂₄H₂₉NO₃

: 1394050-67-9
C₂₉H₃₇NO₅

Guidance literature:: C₂₄H₂₉NO₃; With sodium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 0.75h; Inert atmosphere;

di-tert-butyl dicarbonate; at 5 - 20 ℃; Inert atmosphere;

Reference yield:

: 128779-47-5
(2R)-3-(biphenyl-4-yl)-2-[(tert-butoxycarbonyl)amino]propanoic acid

: 1394050-67-9
C₂₉H₃₇NO₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 9 h / -5 °C / Inert atmosphere

2.1: acetic acid / dichloromethane / 0.5 h / -5 °C / Inert atmosphere

2.2: 2 h / -5 °C / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 23 °C / Inert atmosphere

4.1: hydrogenchloride / cyclopentyl methyl ether / 24 h / 0 - 20 °C / Inert atmosphere

5.1: 2-methyltetrahydrofuran; cyclopentyl methyl ether / 20 °C / Inert atmosphere

6.1: 4-methyl-morpholine / tetrahydrofuran / 0.33 h / 0 - 5 °C / Inert atmosphere

7.1: sodium tetrahydroborate / water; tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

8.1: toluene-4-sulfonic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

9.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.75 h / 0 °C / Inert atmosphere

9.2: 5 - 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; dmap; sodium tetrahydroborate; sodium hexamethyldisilazane; potassium carbonate; acetic acid; dicyclohexyl-carbodiimide; toluene-4-sulfonic acid; In tetrahydrofuran; 2-methyltetrahydrofuran; dichloromethane; cyclopentyl methyl ether; water; N,N-dimethyl-formamide;

Reference yield:

: 1383026-37-6
[(R)-1-biphenyl-4-ylmethyl-2-(2,2-dimethyl-4,6-dioxo-[1,3]dioxan-5-yl)-2-oxoethyl]carbamic acid t-butyl ester

: 1394050-67-9
C₂₉H₃₇NO₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: acetic acid / dichloromethane / 0.5 h / -5 °C / Inert atmosphere

1.2: 2 h / -5 °C / Inert atmosphere

2.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 23 °C / Inert atmosphere

3.1: hydrogenchloride / cyclopentyl methyl ether / 24 h / 0 - 20 °C / Inert atmosphere

4.1: 2-methyltetrahydrofuran; cyclopentyl methyl ether / 20 °C / Inert atmosphere

5.1: 4-methyl-morpholine / tetrahydrofuran / 0.33 h / 0 - 5 °C / Inert atmosphere

6.1: sodium tetrahydroborate / water; tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

7.1: toluene-4-sulfonic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

8.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.75 h / 0 °C / Inert atmosphere

8.2: 5 - 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; sodium tetrahydroborate; sodium hexamethyldisilazane; potassium carbonate; acetic acid; toluene-4-sulfonic acid; In tetrahydrofuran; 2-methyltetrahydrofuran; dichloromethane; cyclopentyl methyl ether; water; N,N-dimethyl-formamide;