Technology Process of 5,5-trimethylene-2,2-diphenyl-1,3-dioxa-5-azonia-2-boratacyclohexane
There total 5 articles about 5,5-trimethylene-2,2-diphenyl-1,3-dioxa-5-azonia-2-boratacyclohexane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
ethanol; water;
A soln. of azetidine in EtOH is mixed with an aq. soln. of formaldehyde, after addn. of oxybisdiphenylborane the mixt. is heated until the soln. becomes clear.; Crystn. begins during the heating or after cooling to room temp., recrystn. fromEtOH, elem. anal..;
- Guidance literature:
-
In
ethanol; water;
A soln. of azetidine in EtOH is mixed with an aq. soln. of formaldehyde, after addn. of (2-aminoethyloxy)diphenylborane the mixt. is heated until the soln. becomes clear.; Crystn. begins during the heating or after cooling to room temp., recrystn. fromEtOH, elem. anal..;
- Guidance literature:
-
In
ethanol; water;
A soln. of azetidine in EtOH is mixed with an aq. soln. of formaldehyde, after addn. of triphenylborane the mixt. is heated until the soln. becomes clear.; Crystn. begins during the heating or after cooling to room temp., recrystn. fromEtOH, elem. anal..;
