N-(5-trimethylsiloxy-5,5-diphenyl-3-pentynyl)-N-(p-toluenesulfonyl)-m-chloroaniline

Base Information

Chemical Name:N-(5-trimethylsiloxy-5,5-diphenyl-3-pentynyl)-N-(p-toluenesulfonyl)-m-chloroaniline
CAS No.:735271-17-7
Molecular Formula:C₃₃H₃₄ClNO₃SSi
Molecular Weight:588.242
Hs Code.:

Synonyms:N-(5-trimethylsiloxy-5,5-diphenyl-3-pentynyl)-N-(p-toluenesulfonyl)-m-chloroaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(5-trimethylsiloxy-5,5-diphenyl-3-pentynyl)-N-(p-toluenesulfonyl)-m-chloroaniline

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Technology Process of N-(5-trimethylsiloxy-5,5-diphenyl-3-pentynyl)-N-(p-toluenesulfonyl)-m-chloroaniline

There total 5 articles about N-(5-trimethylsiloxy-5,5-diphenyl-3-pentynyl)-N-(p-toluenesulfonyl)-m-chloroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: N-(3-chloro-phenyl)-N-(5-hydroxy-5,5-diphenyl-pent-3-ynyl)-4-methyl-benzenesulfonamide

: 735271-17-7
N-(5-trimethylsiloxy-5,5-diphenyl-3-pentynyl)-N-(p-toluenesulfonyl)-m-chloroaniline

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ol049301u

Reference yield:

: 19377-04-9
N-(3-chlorophenyl)-4-methyl-benzenesulfonamide

: 735271-17-7
N-(5-trimethylsiloxy-5,5-diphenyl-3-pentynyl)-N-(p-toluenesulfonyl)-m-chloroaniline

Guidance literature:: Multi-step reaction with 3 steps

1: PPh₃; DEAD / tetrahydrofuran / 20 °C

2: BuLi / tetrahydrofuran / 0 °C

3: imidazole / dimethylformamide / 20 °C

With 1H-imidazole; n-butyllithium; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; N,N-dimethyl-formamide; 1: Mitsunobu reaction;
DOI:10.1021/ol049301u

Reference yield:

: 108-42-9
3-chloro-aniline

: 735271-17-7
N-(5-trimethylsiloxy-5,5-diphenyl-3-pentynyl)-N-(p-toluenesulfonyl)-m-chloroaniline

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / tetrahydrofuran / 20 °C

2: PPh₃; DEAD / tetrahydrofuran / 20 °C

3: BuLi / tetrahydrofuran / 0 °C

4: imidazole / dimethylformamide / 20 °C

With 1H-imidazole; n-butyllithium; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; N,N-dimethyl-formamide; 2: Mitsunobu reaction;
DOI:10.1021/ol049301u