methyl 1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-piperidinecarboxylate

Base Information

Chemical Name:methyl 1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-piperidinecarboxylate
CAS No.:951744-37-9
Molecular Formula:C₃₂H₃₂N₂O₇
Molecular Weight:556.615
Hs Code.:

Synonyms:methyl 1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-piperidinecarboxylate

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Chemical Property of methyl 1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-piperidinecarboxylate

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Technology Process of methyl 1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-piperidinecarboxylate

There total 6 articles about methyl 1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-piperidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 951744-83-5
(1,2-Bis(4-methoxyphenyl)-2-oxoethyl) 1-benzyloxycarbonyl-4-methoxycarbonyl-4-piperidinecarboxylate

: 951744-37-9
methyl 1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-piperidinecarboxylate

Guidance literature:: (1,2-Bis(4-methoxyphenyl)-2-oxoethyl) 1-benzyloxycarbonyl-4-methoxycarbonyl-4-piperidinecarboxylate; With ammonium acetate; acetic acid; at 90 ℃; for 17h;

With sodium hydrogencarbonate; In water; ethyl acetate; Product distribution / selectivity;

Reference yield: 19.0%

: methyl 4,5-bis(4-methoxyphenyl)oxazole-2-acetate

: 189323-09-9
benzyl bis(2-bromoethyl)carbamate

: 951744-37-9
methyl 1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-piperidinecarboxylate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 50 ℃; for 9h; Product distribution / selectivity;

Reference yield:

: 27895-95-0
2-bromo-1,2-bis(4-methoxyphenyl)ethanone

: 951744-37-9
methyl 1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-piperidinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

2: ammonium acetate; acetic acid / 17 h / 90 °C

With ammonium acetate; caesium carbonate; acetic acid; In N,N-dimethyl-formamide;