2,6-di-tert-butyl-4-methylphenyl trans-2-(3-cyclohexen-1-yl)cyclopropanecarboxylate

Base Information

Chemical Name:2,6-di-tert-butyl-4-methylphenyl trans-2-(3-cyclohexen-1-yl)cyclopropanecarboxylate
CAS No.:125640-98-4
Molecular Formula:C₂₅H₃₆O₂
Molecular Weight:368.56
Hs Code.:

Synonyms:2,6-di-tert-butyl-4-methylphenyl trans-2-(3-cyclohexen-1-yl)cyclopropanecarboxylate

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Chemical Property of 2,6-di-tert-butyl-4-methylphenyl trans-2-(3-cyclohexen-1-yl)cyclopropanecarboxylate

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Technology Process of 2,6-di-tert-butyl-4-methylphenyl trans-2-(3-cyclohexen-1-yl)cyclopropanecarboxylate

There total 3 articles about 2,6-di-tert-butyl-4-methylphenyl trans-2-(3-cyclohexen-1-yl)cyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 766-03-0
3-vinylcyclohexene

: 125640-92-8
2,6-di-tert-butyl-4-methylphenyl diazoacetate

: 125640-98-4
2,6-di-tert-butyl-4-methylphenyl trans-2-(3-cyclohexen-1-yl)cyclopropanecarboxylate

Guidance literature:: dirhodium tetraacetate; In dichloromethane; for 2h; Ambient temperature;

Reference yield:

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

: 125640-98-4
2,6-di-tert-butyl-4-methylphenyl trans-2-(3-cyclohexen-1-yl)cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / triethylamine, methanesulfonyl azide / acetonitrile / 1.) reflux, 2.) RT, 7 h

2: 5percent aq. KOH / acetonitrile / 24 h / Ambient temperature

3: 94 percent / Rh₂(OAc)4 / CH₂Cl₂ / 2 h / Ambient temperature

With potassium hydroxide; triethylamine; Methanesulfonyl azide; dirhodium tetraacetate; In dichloromethane; acetonitrile;

Reference yield:

: 125641-00-1
2,6-Bis(1,1-dimethylethyl)-4-methylphenyl 2-diazo-3-butenoate

: 125640-98-4
2,6-di-tert-butyl-4-methylphenyl trans-2-(3-cyclohexen-1-yl)cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 5percent aq. KOH / acetonitrile / 24 h / Ambient temperature

2: 94 percent / Rh₂(OAc)4 / CH₂Cl₂ / 2 h / Ambient temperature

With potassium hydroxide; dirhodium tetraacetate; In dichloromethane; acetonitrile;