benzyl bromo(2-¹³C)acetate

Base Information

Chemical Name:benzyl bromo(2-¹³C)acetate
CAS No.:922182-40-9
Molecular Formula:C₉H₉BrO₂
Molecular Weight:230.062
Hs Code.:

Synonyms:benzyl bromo(2-¹³C)acetate

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Chemical Property of benzyl bromo(2-¹³C)acetate

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Technology Process of benzyl bromo(2-¹³C)acetate

There total 1 articles about benzyl bromo(2-¹³C)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 64891-77-6
(2-13C)bromoacetic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 922182-40-9
benzyl bromo(2-¹³C)acetate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/jo9014497

Reference yield: 97.0%

: 922182-40-9
benzyl bromo(2-¹³C)acetate

: 936831-83-3
benzyl [2-13C]-2-iodoacetate

Guidance literature:: With sodium iodide; In acetone; at 20 ℃; for 1h;
DOI:10.1002/ejoc.200600677

Reference yield: 60.0%

: 922182-40-9
benzyl bromo(2-¹³C)acetate

: 23190-16-1
(1R,2S)-2-Amino-1,2-diphenylethanol

: 501-53-1,94274-21-2
benzyl chloroformate

: 1196980-06-9
[3-⁽¹³⁾C]-(5S,6R)-4-benzyloxycarbonyl-5,6-diphenylmorpholin-2-one

Guidance literature:: benzyl bromo(2-¹³C)acetate; (1R,2S)-2-Amino-1,2-diphenylethanol; With triethylamine; In tetrahydrofuran; at 20 ℃; for 4h;

benzyl chloroformate; With sodium hydrogencarbonate; In dichloromethane; water; at 0 ℃; for 2.33333h;

With toluene-4-sulfonic acid; In toluene; Reflux;
DOI:10.1021/jo9014497