(1R,2R,4R)-4-hydroxy-cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester

Base Information

Chemical Name:(1R,2R,4R)-4-hydroxy-cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester
CAS No.:1265882-90-3
Molecular Formula:C₁₆H₂₀O₅
Molecular Weight:292.332
Hs Code.:

Synonyms:(1R,2R,4R)-4-hydroxy-cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester

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Chemical Property of (1R,2R,4R)-4-hydroxy-cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester

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Technology Process of (1R,2R,4R)-4-hydroxy-cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester

There total 6 articles about (1R,2R,4R)-4-hydroxy-cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1265882-89-0,188796-05-6
(1R,2R,5R)-7-oxo-6-oxabicyclo[3,2,1]octane-2-carboxylic acid methyl ester

: 100-51-6,185532-71-2
benzyl alcohol

: 1265882-90-3
(1R,2R,4R)-4-hydroxy-cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 16h; Inert atmosphere;

Reference yield: 70.0%

: 1265882-89-0,188796-05-6
(1R,2R,5R)-7-oxo-6-oxabicyclo[3,2,1]octane-2-carboxylic acid methyl ester

: 1265882-90-3
(1R,2R,4R)-4-hydroxy-cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester

: 1265883-85-9
(1R,2R,4R)-4-(tert-butyldiphenylsilanyloxy)cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester

Guidance literature:: With potassium carbonate; benzyl alcohol; In N,N-dimethyl-formamide;

Reference yield:

: 323196-38-9
(1R,2R)-cyclohex-4-ene 1,2-dicarboxylic acid monomethyl ester

: 1265882-90-3
(1R,2R,4R)-4-hydroxy-cyclohexane-1,2-dicarboxylic acid 2-benzyl ester 1-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium iodide; sodium hydrogencarbonate; iodine / dichloromethane; water / 48 h

2: tris-(trimethylsilyl)silane / 2,2'-azobis(isobutyronitrile) / toluene / 1.5 h / 90 °C

3: potassium carbonate / N,N-dimethyl-formamide / 16 h / Inert atmosphere

With tris-(trimethylsilyl)silane; iodine; sodium hydrogencarbonate; potassium carbonate; potassium iodide; 2,2'-azobis(isobutyronitrile); In dichloromethane; water; N,N-dimethyl-formamide; toluene;