(4-Chloro-phenylamino)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

Base Information

• Chemical Name: (4-Chloro-phenylamino)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide
• CAS No.: 93548-64-2
• Molecular Formula: C₁₆H₁₆ClN₃O₂
• Molecular Weight: 317.775

Synonyms:(4-Chloro-phenylamino)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

Chemical Property of (4-Chloro-phenylamino)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

Chemical Property:

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Technology Process of (4-Chloro-phenylamino)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

There total 1 articles about (4-Chloro-phenylamino)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

2-((4-chlorophenyl)amino)acetohydrazide (2371-31-5) + 4-methoxy-benzaldehyde (123-11-5) → (4-Chloro-phenylamino)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide (93548-64-2)

Guidance literature:

With acetic acid; In benzene; for 6h; Heating;

DOI:10.1002/ardp.19843171015

Reference yield: 44.0%

(4-Chloro-phenylamino)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide (93548-64-2) → (4-Chloro-phenylamino)-acetic acid N'-(4-methoxy-benzyl)-hydrazide (93548-70-0)

Guidance literature:

With hydrazine hydrate; palladium on activated charcoal; In N,N-dimethyl-formamide; for 8h; Heating;

DOI:10.1002/ardp.19843171015

Reference yield: 37.0%

(4-Chloro-phenylamino)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide (93548-64-2) + chloroacetyl chloride (79-04-9) → N-[3-Chloro-2-(4-methoxy-phenyl)-4-oxo-azetidin-1-yl]-2-(4-chloro-phenylamino)-acetamide (93548-75-5)

Guidance literature:

for 3h; Heating;

DOI:10.1002/ardp.19843171015

upstream raw materials:

2-((4-chlorophenyl)amino)acetohydrazide

4-methoxy-benzaldehyde

Downstream raw materials:

(4-Chloro-phenylamino)-acetic acid N'-(4-methoxy-benzyl)-hydrazide

N-[3-Chloro-2-(4-methoxy-phenyl)-4-oxo-azetidin-1-yl]-2-(4-chloro-phenylamino)-acetamide

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