1,1-Dimethylethyl N-acetyl-N-(2-bromophenyl)carbamate

Base Information

Chemical Name:1,1-Dimethylethyl N-acetyl-N-(2-bromophenyl)carbamate
CAS No.:947494-79-3
Molecular Formula:C₁₃H₁₆BrNO₃
Molecular Weight:314.179
Hs Code.:
DSSTox Substance ID:DTXSID901214324

Synonyms:1,1-Dimethylethyl N-acetyl-N-(2-bromophenyl)carbamate;DTXSID901214324;947494-79-3

Suppliers and Price of 1,1-Dimethylethyl N-acetyl-N-(2-bromophenyl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-Dimethylethyl N-acetyl-N-(2-bromophenyl)carbamate

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:313.03136
Heavy Atom Count:18
Complexity:325

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)N(C1=CC=CC=C1Br)C(=O)OC(C)(C)C

Technology Process of 1,1-Dimethylethyl N-acetyl-N-(2-bromophenyl)carbamate

There total 2 articles about 1,1-Dimethylethyl N-acetyl-N-(2-bromophenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 614-76-6
N-acetyl-2-bromoaniline

: 947494-79-3
C₁₃H₁₆BrNO₃

Guidance literature:: With dmap; In tetrahydrofuran; at 20 ℃; for 0.833333h;
DOI:10.1021/jo801985a

Reference yield:

: 615-36-1
2-bromoaniline

: 947494-79-3
C₁₃H₁₆BrNO₃

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 °C

2: dmap / 25 °C

With dmap; triethylamine; In dichloromethane;
DOI:10.1155/2017/8418939

Reference yield: 78.0%

: 947494-79-3
C₁₃H₁₆BrNO₃

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 947494-80-6
C₂₅H₂₅NPO₆Br

Guidance literature:: C₁₃H₁₆BrNO₃; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h;

chlorophosphoric acid diphenyl ester; In tetrahydrofuran; at -78 ℃; for 1h;
DOI:10.1155/2017/8418939