di(pentachlorophenolato)triphenylantimony(V)

Base Information

Chemical Name:di(pentachlorophenolato)triphenylantimony(V)
CAS No.:17363-17-6
Molecular Formula:C₃₀H₁₅Cl₁₀O₂Sb
Molecular Weight:883.728
Hs Code.:

Synonyms:di(pentachlorophenolato)triphenylantimony(V)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(pentachlorophenolato)triphenylantimony(V)

Chemical Property:

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Technology Process of di(pentachlorophenolato)triphenylantimony(V)

There total 3 articles about di(pentachlorophenolato)triphenylantimony(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 87-86-5,67471-28-7
Pentachlorophenol

: 603-36-1
triphenylantimony

: 17363-17-6
di(pentachlorophenolato)triphenylantimony(V)

Guidance literature:: With tert.-butylhydroperoxide; In diethyl ether; at 20 ℃; for 24h;
DOI:10.1134/S0036023617100163

Reference yield: 80.6%

: 87-86-5,67471-28-7
Pentachlorophenol

: 1538-59-6,20265-30-9,34716-92-2
triphenylantimony dibromide

: 17363-17-6
di(pentachlorophenolato)triphenylantimony(V)

Guidance literature:: With triethylamine; In benzene; byproducts: Et3NHBr; 2 equiv. Cl5C6OH and Et3N are stirred in dry benzene at 25-30 °Cfor about 1 h, refluxed for about 2 h; Et3NHBr was filtered off, the filtrate was concd., petroleum ether was added, recrystd. (benzene/petroleum ether); elem. anal.;

Reference yield: 66.4%

: 1538-59-6,20265-30-9,34716-92-2
triphenylantimony dibromide

: 131-52-2
sodium pentachlorphenate

: 17363-17-6
di(pentachlorophenolato)triphenylantimony(V)

Guidance literature:: In benzene; byproducts: NaBr; 2 equiv. Cl5C6ONa are refluxed in dry benzene for about 4 h; NaBr was filtered off, the filtrate was concd., petroleum ether was added, recrystd. (benzene/petroleum ether); elem. anal.;