cyclohexyl {4-[3-chloro-2-(4-methoxyphenyl)-4-oxoazetidin-1-yl]phenyl}carbamate

Base Information

Chemical Name:cyclohexyl {4-[3-chloro-2-(4-methoxyphenyl)-4-oxoazetidin-1-yl]phenyl}carbamate
CAS No.:1450735-86-0
Molecular Formula:C₂₃H₂₅ClN₂O₄
Molecular Weight:428.915
Hs Code.:

Synonyms:cyclohexyl {4-[3-chloro-2-(4-methoxyphenyl)-4-oxoazetidin-1-yl]phenyl}carbamate

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Chemical Property of cyclohexyl {4-[3-chloro-2-(4-methoxyphenyl)-4-oxoazetidin-1-yl]phenyl}carbamate

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Technology Process of cyclohexyl {4-[3-chloro-2-(4-methoxyphenyl)-4-oxoazetidin-1-yl]phenyl}carbamate

There total 2 articles about cyclohexyl {4-[3-chloro-2-(4-methoxyphenyl)-4-oxoazetidin-1-yl]phenyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1450735-85-9
cyclohexyl {4-[(4-methoxyphenyl)methylidene]aminophenyl}carbamate

: 79-04-9
chloroacetyl chloride

: 1450735-86-0
cyclohexyl {4-[3-chloro-2-(4-methoxyphenyl)-4-oxoazetidin-1-yl]phenyl}carbamate

Guidance literature:: cyclohexyl {4-[(4-methoxyphenyl)methylidene]aminophenyl}carbamate; chloroacetyl chloride; In 1,4-dioxane; at 20 ℃; for 0.166667h;

With triethylamine; In 1,4-dioxane; for 12h; Reflux;
DOI:10.1134/S1070428013070087

Reference yield:

: 20995-16-8
cyclohexyl N-(4-aminophenyl)carbamate

: 123-11-5
4-methoxy-benzaldehyde

: 1450735-86-0
cyclohexyl {4-[3-chloro-2-(4-methoxyphenyl)-4-oxoazetidin-1-yl]phenyl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / ethanol / 5 h / Reflux

2.1: 1,4-dioxane / 0.17 h / 20 °C

2.2: 12 h / Reflux

With acetic acid; In 1,4-dioxane; ethanol;
DOI:10.1134/S1070428013070087