N-(4-(methoxycarbonyl)-1-butenyl)-N-(p-toluenesulfonyl)-2-ethenylaniline

Base Information

Chemical Name:N-(4-(methoxycarbonyl)-1-butenyl)-N-(p-toluenesulfonyl)-2-ethenylaniline
CAS No.:894810-73-2
Molecular Formula:C₂₁H₂₃NO₄S
Molecular Weight:385.484
Hs Code.:

Synonyms:N-(4-(methoxycarbonyl)-1-butenyl)-N-(p-toluenesulfonyl)-2-ethenylaniline

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Chemical Property of N-(4-(methoxycarbonyl)-1-butenyl)-N-(p-toluenesulfonyl)-2-ethenylaniline

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Technology Process of N-(4-(methoxycarbonyl)-1-butenyl)-N-(p-toluenesulfonyl)-2-ethenylaniline

There total 4 articles about N-(4-(methoxycarbonyl)-1-butenyl)-N-(p-toluenesulfonyl)-2-ethenylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 876392-11-9
N-(4-(methoxycarbonyl)-3-butenyl)-N-(p-toluenesulfonyl)-2-ethenylaniline

: 894810-73-2
N-(4-(methoxycarbonyl)-1-butenyl)-N-(p-toluenesulfonyl)-2-ethenylaniline

Guidance literature:: (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); In toluene; for 15h; Heating;
DOI:10.1021/jo060308u

Reference yield: 52.0%

: 876392-11-9
N-(4-(methoxycarbonyl)-3-butenyl)-N-(p-toluenesulfonyl)-2-ethenylaniline

: 894810-73-2
N-(4-(methoxycarbonyl)-1-butenyl)-N-(p-toluenesulfonyl)-2-ethenylaniline

: 876392-15-3
N-(p-toluenesulfonyl)-2-(3-(methoxycarbonyl)propyl)-3-methylene-2,3-dihydroindole

Guidance literature:: With trimethylsiloxyethene; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In xylene; for 2h; Heating;
DOI:10.1021/jo060308u

Reference yield:

: 30765-95-8
N-p-toluenesulfonyl-2-vinylaniline

: 894810-73-2
N-(4-(methoxycarbonyl)-1-butenyl)-N-(p-toluenesulfonyl)-2-ethenylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran; toluene / 4 h / 20 °C

2: 83 percent / RuClH(CO)(PPh₃)3 / toluene / 15 h / Heating

With triphenylphosphine; diethylazodicarboxylate; (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); In tetrahydrofuran; toluene;
DOI:10.1021/jo060308u