2-bromomethyl-acrylic acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester

Base Information

• Chemical Name: 2-bromomethyl-acrylic acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester
• CAS No.: 1000170-44-4
• Molecular Formula: C₁₀H₆BrF₁₁O₂
• Molecular Weight: 447.043

Synonyms:2-bromomethyl-acrylic acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester

Chemical Property of 2-bromomethyl-acrylic acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester

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Technology Process of 2-bromomethyl-acrylic acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester

There total 1 articles about 2-bromomethyl-acrylic acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

perfluorohexanol (423-46-1) + 2-(bromomethyl)acrylic acid (72707-66-5) → 2-bromomethyl-acrylic acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester (1000170-44-4)

Guidance literature:

With sulfuric acid; at 50 - 130 ℃; for 6.25h;

DOI:10.1039/b713244c

Reference yield: 90.0%

2-bromomethyl-acrylic acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester (1000170-44-4) + 4-methoxy-benzaldehyde (123-11-5) → 4-hydroxy-4-(4-methoxy-phenyl)-2-methylene-butyric acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester (1000170-54-6)

Guidance literature:

With indium; air; In water; at 20 ℃; for 24h;

DOI:10.1039/b713244c

Reference yield: 86.0%

2-bromomethyl-acrylic acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester (1000170-44-4) + benzaldehyde (100-52-7) → 4-hydroxy-2-methylene-4-phenyl-butyric acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester (1000170-45-5)

Guidance literature:

With indium; air; In water; at 20 ℃; for 24h;

DOI:10.1039/b713244c

upstream raw materials:

perfluorohexanol

2-(bromomethyl)acrylic acid

Downstream raw materials:

4-(3,4-difluoro-phenyl)-4-hydroxy-2-methylene-butyric acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester

4-(4-fluoro-phenyl)-4-hydroxy-2-methylene-butyric acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester

4-(4-chloro-phenyl)-4-hydroxy-2-methylene-butyric acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester

4-hydroxy-2-methylene-4-phenyl-butyric acid 2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyl ester

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