2,2,2-trifluoro-1-(2-fluoro-5-(4-fluorobenzoyl)phenyl)ethanone

Base Information

Chemical Name:2,2,2-trifluoro-1-(2-fluoro-5-(4-fluorobenzoyl)phenyl)ethanone
CAS No.:1599529-26-6
Molecular Formula:C₁₅H₇F₅O₂
Molecular Weight:314.211
Hs Code.:

Synonyms:2,2,2-trifluoro-1-(2-fluoro-5-(4-fluorobenzoyl)phenyl)ethanone

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Chemical Property of 2,2,2-trifluoro-1-(2-fluoro-5-(4-fluorobenzoyl)phenyl)ethanone

Chemical Property:

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Technology Process of 2,2,2-trifluoro-1-(2-fluoro-5-(4-fluorobenzoyl)phenyl)ethanone

There total 3 articles about 2,2,2-trifluoro-1-(2-fluoro-5-(4-fluorobenzoyl)phenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1599529-24-4
2,2,2-trifluoro-1-(2-fluoro-5-((4-fluorophenyl)(hydroxy)methyl)phenyl)ethanone

: 1599529-26-6
2,2,2-trifluoro-1-(2-fluoro-5-(4-fluorobenzoyl)phenyl)ethanone

Guidance literature:: With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide; In dichloromethane; water; for 0.416667h; Cooling with ice;

Reference yield:

: 227609-88-3
4-fluoro-3-iodobenzaldehyde

: 1599529-26-6
2,2,2-trifluoro-1-(2-fluoro-5-(4-fluorobenzoyl)phenyl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 0.11 h / 20 °C / Cooling with acetone-dry ice; Inert atmosphere

1.2: 0.54 h / Cooling with acetone-dry ice; Inert atmosphere

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite; potassium bromide; sodium hydrogencarbonate / dichloromethane; water / 0.42 h / Cooling with ice

With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide; In tetrahydrofuran; dichloromethane; water;

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 1599529-26-6
2,2,2-trifluoro-1-(2-fluoro-5-(4-fluorobenzoyl)phenyl)ethanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic anhydride; sodium periodate; potassium iodide; sulfuric acid / 0.01 h / 20 °C

1.2: 21 h / 20 - 30 °C

2.1: tetrahydrofuran / 0.11 h / 20 °C / Cooling with acetone-dry ice; Inert atmosphere

2.2: 0.54 h / Cooling with acetone-dry ice; Inert atmosphere

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite; potassium bromide; sodium hydrogencarbonate / dichloromethane; water / 0.42 h / Cooling with ice

With sodium hypochlorite; sodium periodate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sulfuric acid; acetic anhydride; sodium hydrogencarbonate; potassium iodide; potassium bromide; In tetrahydrofuran; dichloromethane; water;