(R,R)-N,N'-(cyclohexane-1,2-diyl)bis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

Base Information

Chemical Name:(R,R)-N,N'-(cyclohexane-1,2-diyl)bis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>
CAS No.:223704-18-5
Molecular Formula:C₂₈H₄₂N₂O₁₀S₄
Molecular Weight:694.913
Hs Code.:

Synonyms:(R,R)-N,N'-(cyclohexane-1,2-diyl)bis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,R)-N,N'-(cyclohexane-1,2-diyl)bis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

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Technology Process of (R,R)-N,N'-(cyclohexane-1,2-diyl)bis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

There total 6 articles about (R,R)-N,N'-(cyclohexane-1,2-diyl)bis-<3-(p-toluenesulphonylamino)propyl methanesulphonate> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 124-63-0
methanesulfonyl chloride

: 223704-16-3
(R,R)-N,N'-(cyclohexane-1,2-diyl)bis-<3-(p-toluenesulfonylamino)propan-1-ol>

: 223704-18-5
(R,R)-N,N'-(cyclohexane-1,2-diyl)bis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

Guidance literature:: With pyridine; In acetonitrile; at 0 ℃; for 1.5h;
DOI:10.1016/S0957-4166(99)00010-5

Reference yield:

: 143585-47-1
(R,R)-1,2-bis(tosylamino)cyclohexane

: 223704-18-5
(R,R)-N,N'-(cyclohexane-1,2-diyl)bis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / K₂CO₃ / acetonitrile / 48 h / 70 °C

2: triethylamine / CH₂Cl₂ / 0 °C

With potassium carbonate; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1002/ejoc.200600234

Reference yield:

: 852043-14-2
C₆₄H₆₆N₂O₆S₂

: 223704-18-5
(R,R)-N,N'-(cyclohexane-1,2-diyl)bis-<3-(p-toluenesulphonylamino)propyl methanesulphonate>

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / CH₂Cl₂; methanol

2: triethylamine / CH₂Cl₂ / 0 °C

With triethylamine; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1002/ejoc.200600234