C₁₅H₁₅F₂NO₃S

Base Information

Chemical Name:C₁₅H₁₅F₂NO₃S
CAS No.:1204424-03-2
Molecular Formula:C₁₅H₁₅F₂NO₃S
Molecular Weight:327.352
Hs Code.:

C<sub>15</sub>H<sub>15</sub>F<sub>2</sub>NO<sub>3</sub>S

Synonyms:C₁₅H₁₅F₂NO₃S

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Chemical Property of C₁₅H₁₅F₂NO₃S

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Technology Process of C₁₅H₁₅F₂NO₃S

There total 5 articles about C₁₅H₁₅F₂NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 7648-30-8
ethyl 2,2-difluoro-2-iodoacetate

: 1204423-52-8
5-Bromomethyl-2-(4-methoxyphenyl)-thiazole

: 1204424-03-2
C₁₅H₁₅F₂NO₃S

Guidance literature:: ethyl 2,2-difluoro-2-iodoacetate; With copper; In dimethyl sulfoxide; at 20 ℃; for 0.5h;

5-Bromomethyl-2-(4-methoxyphenyl)-thiazole; In dimethyl sulfoxide; for 0.25h;

Reference yield:

: 5720-07-0
4-methoxyphenylboronic acid

: 1204424-03-2
C₁₅H₁₅F₂NO₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / triphenylphosphine; palladium diacetate / N,N-dimethyl-formamide; water / 3 h / 100 °C

2.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C

2.2: 0 °C

3.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 0 °C

4.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 20 °C

5.1: copper / dimethyl sulfoxide / 0.5 h / 20 °C

5.2: 0.25 h

With methanol; sodium tetrahydroborate; n-butyllithium; carbon tetrabromide; copper; sodium carbonate; triphenylphosphine; palladium diacetate; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 27088-84-2
2-(4-methoxyphenyl)-1,3-thiazole

: 1204424-03-2
C₁₅H₁₅F₂NO₃S

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C

1.2: 0 °C

2.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 0 °C

3.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 20 °C

4.1: copper / dimethyl sulfoxide / 0.5 h / 20 °C

4.2: 0.25 h

With methanol; sodium tetrahydroborate; n-butyllithium; carbon tetrabromide; copper; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide;