3-[4-(2-{[6-({2-[4-(2-Carboxy-2-ethoxy-ethyl)-phenylsulfanyl]-ethyl}-methyl-amino)-pyridin-2-yl]-methyl-amino}-ethylsulfanyl)-phenyl]-2-ethoxy-propionic acid

Base Information

Chemical Name:3-[4-(2-{[6-({2-[4-(2-Carboxy-2-ethoxy-ethyl)-phenylsulfanyl]-ethyl}-methyl-amino)-pyridin-2-yl]-methyl-amino}-ethylsulfanyl)-phenyl]-2-ethoxy-propionic acid
CAS No.:719293-24-0
Molecular Formula:C₃₃H₄₃N₃O₆S₂
Molecular Weight:641.853
Hs Code.:

3-[4-(2-{[6-({2-[4-(2-Carboxy-2-ethoxy-ethyl)-phenylsulfanyl]-ethyl}-methyl-amino)-pyridin-2-yl]-methyl-amino}-ethylsulfanyl)-phenyl]-2-ethoxy-propionic acid

Synonyms:3-[4-(2-{[6-({2-[4-(2-Carboxy-2-ethoxy-ethyl)-phenylsulfanyl]-ethyl}-methyl-amino)-pyridin-2-yl]-methyl-amino}-ethylsulfanyl)-phenyl]-2-ethoxy-propionic acid

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Chemical Property of 3-[4-(2-{[6-({2-[4-(2-Carboxy-2-ethoxy-ethyl)-phenylsulfanyl]-ethyl}-methyl-amino)-pyridin-2-yl]-methyl-amino}-ethylsulfanyl)-phenyl]-2-ethoxy-propionic acid

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Technology Process of 3-[4-(2-{[6-({2-[4-(2-Carboxy-2-ethoxy-ethyl)-phenylsulfanyl]-ethyl}-methyl-amino)-pyridin-2-yl]-methyl-amino}-ethylsulfanyl)-phenyl]-2-ethoxy-propionic acid

There total 11 articles about 3-[4-(2-{[6-({2-[4-(2-Carboxy-2-ethoxy-ethyl)-phenylsulfanyl]-ethyl}-methyl-amino)-pyridin-2-yl]-methyl-amino}-ethylsulfanyl)-phenyl]-2-ethoxy-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 719293-23-9
2-ethoxy-3-[4-(2-{[6-({2-[4-(2-ethoxy-2-methoxycarbonyl-ethyl)-phenylsulfanyl]-ethyl}-methyl-amino)-pyridin-2-yl]-methyl-amino}-ethylsulfanyl)-phenyl]-propionic acid methyl ester

: 719293-24-0
3-[4-(2-{[6-({2-[4-(2-Carboxy-2-ethoxy-ethyl)-phenylsulfanyl]-ethyl}-methyl-amino)-pyridin-2-yl]-methyl-amino}-ethylsulfanyl)-phenyl]-2-ethoxy-propionic acid

Guidance literature:: With sodium hydroxide; water; In ethanol; at 60 ℃; for 5h; Heating / reflux;

Reference yield:

: 22121-91-1
ethyl α-ethoxycinnamate

: 719293-24-0
3-[4-(2-{[6-({2-[4-(2-Carboxy-2-ethoxy-ethyl)-phenylsulfanyl]-ethyl}-methyl-amino)-pyridin-2-yl]-methyl-amino}-ethylsulfanyl)-phenyl]-2-ethoxy-propionic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen / 5%-palladium/activated carbon / ethanol / 20 °C / 7600.51 Torr

2.1: chlorosulfonic acid / 1.33 h / -2 - 0 °C

3.1: hydrogenchloride; tin / 3.33 h / Heating / reflux

4.1: tributylphosphine / tetrahydrofuran / 0.25 h / 0 °C

4.2: 6 h

5.1: sodium hydroxide; water / ethanol / 5 h / 60 °C / Heating / reflux

With hydrogenchloride; chlorosulfonic acid; sodium hydroxide; tin; tributylphosphine; water; hydrogen; 5%-palladium/activated carbon; In tetrahydrofuran; ethanol;

Reference yield:

: 197299-16-4
ethyl 2-ethoxy-3-(4-hydroxy-phenyl)-propionate

: 719293-24-0
3-[4-(2-{[6-({2-[4-(2-Carboxy-2-ethoxy-ethyl)-phenylsulfanyl]-ethyl}-methyl-amino)-pyridin-2-yl]-methyl-amino}-ethylsulfanyl)-phenyl]-2-ethoxy-propionic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dmap / 1,4-dioxane / 10 h / 100 °C / Heating / reflux

2.1: tetradecane / 8 h / 230 - 245 °C / Heating / reflux

3.1: methanol; potassium hydroxide / tetrahydrofuran / 15 h / 10 - 20 °C

4.1: hydrogenchloride / benzene / 30 - 35 °C

5.1: tributylphosphine / tetrahydrofuran / 0.25 h / 0 °C

5.2: 6 h

6.1: sodium hydroxide; water / ethanol / 5 h / 60 °C / Heating / reflux

With hydrogenchloride; methanol; potassium hydroxide; sodium hydroxide; tributylphosphine; water; triethylamine; dmap; In tetrahydrofuran; 1,4-dioxane; ethanol; tetradecane; benzene;