2,4,6-trinitrophenylacetophenone

Base Information

• Chemical Name: 2,4,6-trinitrophenylacetophenone
• CAS No.: 35113-74-7
• Molecular Formula: C₁₄H₉N₃O₇
• Molecular Weight: 331.241

Synonyms:2,4,6-trinitrophenylacetophenone

Chemical Property of 2,4,6-trinitrophenylacetophenone

Chemical Property:

Purity/Quality:

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Technology Process of 2,4,6-trinitrophenylacetophenone

There total 6 articles about 2,4,6-trinitrophenylacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.5%

C14H10N3O7(1-)*C6H15N*H(1+) (72318-42-4) → 2,4,6-trinitrophenylacetophenone (35113-74-7)

Guidance literature:

With ammonium cerium(IV) nitrate; In water; acetonitrile; for 2.5h; Ambient temperature;

DOI:10.1021/jo9518617

Reference yield:

naphthalene; compound with 2-chloro-1,3,5-trinitro-benzene (21416-60-4) → 2,4,6-trinitrophenylacetophenone (35113-74-7)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanolic sodium ethylate

With sodium ethanolate;

Reference yield:

ethyl 3-oxo-3-phenylpropionate (94-02-0) → 2,4,6-trinitrophenylacetophenone (35113-74-7)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanolic sodium ethylate

With sodium ethanolate;

upstream raw materials:

3-oxo-3-phenyl-2-picryl-propionic acid ethyl ester

1,3,5-trinitrobenzene

acetophenone

C₁₄H₁₀N₃O₇^(1-)*C₆H₁₅N*H⁽¹⁺⁾

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