2,2,2-trichloroethyl 7β-phenylacetamido-2-methylene-3-methyl-3-cephem-4-carboxylate 1-oxide

Base Information

Chemical Name:2,2,2-trichloroethyl 7β-phenylacetamido-2-methylene-3-methyl-3-cephem-4-carboxylate 1-oxide
CAS No.:61365-01-3
Molecular Formula:C₁₉H₁₇Cl₃N₂O₅S
Molecular Weight:491.779
Hs Code.:

Synonyms:2,2,2-trichloroethyl 7β-phenylacetamido-2-methylene-3-methyl-3-cephem-4-carboxylate 1-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2,2-trichloroethyl 7β-phenylacetamido-2-methylene-3-methyl-3-cephem-4-carboxylate 1-oxide

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Technology Process of 2,2,2-trichloroethyl 7β-phenylacetamido-2-methylene-3-methyl-3-cephem-4-carboxylate 1-oxide

There total 2 articles about 2,2,2-trichloroethyl 7β-phenylacetamido-2-methylene-3-methyl-3-cephem-4-carboxylate 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 33465-39-3
2,2,2-trichloroethyl 7β-phenylacetamido-3-methyl-3-cephem-4-carboxylate 1S-(β)-oxide

: 61365-01-3
2,2,2-trichloroethyl 7β-phenylacetamido-2-methylene-3-methyl-3-cephem-4-carboxylate 1-oxide

Guidance literature:: With N,N-dimethylammonium chloride; In dichloromethane; butan-1-ol; for 24h; Heating;

Reference yield:

: 28180-80-5
(6R,7R)-2,2,2-trichloroethyl 3-methyl-7-phenylacetamidoceph-3-em-4-carboxylate

: 61365-01-3
2,2,2-trichloroethyl 7β-phenylacetamido-2-methylene-3-methyl-3-cephem-4-carboxylate 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloroperbenzoic acid / CH₂Cl₂ / 3 h / Ambient temperature

2: 88 percent / dimethylamine hydrochloride / CH₂Cl₂; butan-1-ol / 24 h / Heating

With N,N-dimethylammonium chloride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; butan-1-ol;