Triphenoxyboroxin

Base Information

Chemical Name:Triphenoxyboroxin
CAS No.:7187-84-0
Molecular Formula:C₁₈H₁₅B₃O₆
Molecular Weight:359.746
Hs Code.:
European Community (EC) Number:615-679-4
DSSTox Substance ID:DTXSID101313645

Synonyms:triphenoxyboroxin;2,4,6-Triphenoxyboroxin;SCHEMBL7742431;DTXSID101313645;7187-84-0

Suppliers and Price of Triphenoxyboroxin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Triphenoxyboroxin

Chemical Property:

Vapor Pressure:1.48E-06mmHg at 25°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:360.1147787
Heavy Atom Count:27
Complexity:354

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(OB(OB(O1)OC2=CC=CC=C2)OC3=CC=CC=C3)OC4=CC=CC=C4

Technology Process of Triphenoxyboroxin

There total 9 articles about Triphenoxyboroxin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1095-03-0
triphenylborane

: 11113-50-1,14635-83-7
boric acid

: 7187-84-0
triphenoxyboroxine

Guidance literature:: With calcium hydride; In cyclohexane; react. under N2, suspending the trialkoxyborane , B(OH)3 and CaH2 in cyclohexane, stirring for 1 h at room temp., heating to 80-90°C overnight; hot filtration under N2, washing with hot toluene, evapn.;

Reference yield: 81.0%

: 11113-50-1,14635-83-7
boric acid

: 108-95-2,27073-41-2
phenol

: 7187-84-0
triphenoxyboroxine

Guidance literature:: With calcium hydride; In cyclohexane; byproducts: H2; react. under N2, slow addn. of the alcohol via syringe to B(OH)3 (ratio 1:1) and CaH2, cooling in a water bath, slow heating to 80-90°C for 24 h after abating the H2 gas evolution; hot filtration under N2, extn. with hot cyclohexane or toluene, evapn.;