C₁₇H₂₉NO₅SSi

Base Information

Chemical Name:C₁₇H₂₉NO₅SSi
CAS No.:1028432-16-7
Molecular Formula:C₁₇H₂₉NO₅SSi
Molecular Weight:387.572
Hs Code.:

C<sub>17</sub>H<sub>29</sub>NO<sub>5</sub>SSi

Synonyms:C₁₇H₂₉NO₅SSi

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Chemical Property of C₁₇H₂₉NO₅SSi

Chemical Property:

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Technology Process of C₁₇H₂₉NO₅SSi

There total 3 articles about C₁₇H₂₉NO₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 547-64-8,2155-30-8
methyl lactate

: 1028432-04-3
N-(tert-butyldimethylsilyloxy)-4-methylbenzenesulfonamide

: 1028432-16-7
C₁₇H₂₉NO₅SSi

Guidance literature:: methyl lactate; N-(tert-butyldimethylsilyloxy)-4-methylbenzenesulfonamide; With triphenylphosphine; In tetrahydrofuran; toluene; for 0.166667h; Inert atmosphere; Cooling with ice;

With diethylazodicarboxylate; In tetrahydrofuran; toluene; at 0 - 10 ℃; Inert atmosphere;
DOI:10.15227/orgsyn.089.0480

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1028432-16-7
C₁₇H₂₉NO₅SSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxylamine hydrochloride / N,N-dimethyl-formamide / 0.5 h / Cooling with ice

1.2: 10 °C

1.3: 10 °C

2.1: triphenylphosphine / toluene; tetrahydrofuran / 0.17 h / Inert atmosphere; Cooling with ice

2.2: 0 - 10 °C / Inert atmosphere

With hydroxylamine hydrochloride; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 2.1: |Mitsunobu Displacement / 2.2: |Mitsunobu Displacement;
DOI:10.15227/orgsyn.089.0480

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1028432-16-7
C₁₇H₂₉NO₅SSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxylamine hydrochloride / N,N-dimethyl-formamide / 0.5 h / Cooling with ice

1.2: 10 °C

1.3: 10 °C

2.1: triphenylphosphine / toluene; tetrahydrofuran / 0.17 h / Inert atmosphere; Cooling with ice

2.2: 0 - 10 °C / Inert atmosphere

With hydroxylamine hydrochloride; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 2.1: |Mitsunobu Displacement / 2.2: |Mitsunobu Displacement;
DOI:10.15227/orgsyn.089.0480