phenylphosphine pentacarbonyltungsten⁽⁰⁾

Base Information

Chemical Name:phenylphosphine pentacarbonyltungsten⁽⁰⁾
CAS No.:61300-75-2
Molecular Formula:C₁₁H₇O₅PW
Molecular Weight:433.997
Hs Code.:

phenylphosphine pentacarbonyltungsten<sup>(0)</sup>

Synonyms:phenylphosphine pentacarbonyltungsten⁽⁰⁾

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylphosphine pentacarbonyltungsten⁽⁰⁾

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Technology Process of phenylphosphine pentacarbonyltungsten⁽⁰⁾

There total 14 articles about phenylphosphine pentacarbonyltungsten⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.2%

: 1350883-58-7,1350883-63-4
[(W(CO)5)2(PhPHPHPh)]

: 1333-74-0
hydrogen

: 61300-75-2
phenylphosphine pentacarbonyltungsten⁽⁰⁾

Guidance literature:: In toluene; High Pressure; exposure of tungsten compd. in toluene to 20 bar of H2, heating at 150°C for 3 h; cooling to room temp., evapn., chromy. (silica gel, 90/10 hexane/CH2Cl2)at 0°C;
DOI:10.1021/om2009974

Reference yield: 45.0%

: 82839-08-5
(phenylphosphinous acid)pentacarbonyltungsten

: 1333-74-0
hydrogen

: 61300-75-2
phenylphosphine pentacarbonyltungsten⁽⁰⁾

Guidance literature:: In toluene; High Pressure; exposure of tungsten compd. in toluene to 20 bar of H2, heating at 150°C for 10 h; cooling to room temp., evapn., chromy. (silica gel, 90/10 hexane/CH2Cl2)at -5°C;
DOI:10.1021/om2009974

Reference yield: 44.0%

: 82839-15-4
chlorophenylphosphine-pentacarbonyl-tungsten⁽⁰⁾=Chlorophenylphosphin-pentacarbonyl-wolfram⁽⁰⁾

: 61300-75-2
phenylphosphine pentacarbonyltungsten⁽⁰⁾

: 18461-46-6
PhPCl₂W(CO)5

Guidance literature:: With aluminium trichloride; In dichloromethane; W complex treated with AlCl3 in CH2Cl2 at room temp. under Ar for 3 h, mixture hydrolyzed; evapn., chromy. (SiO2, hexane);