Technology Process of C17H17NO3S
There total 4 articles about C17H17NO3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine;
In
N,N-dimethyl-formamide;
at 50 ℃;
for 19h;
Inert atmosphere;
DOI:10.1021/ja4047069
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / Inert atmosphere
2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
1: |Mitsunobu Displacement / 2: |Sonogashira Cross-Coupling;
DOI:10.1002/chem.201301599
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Schlenk technique; Sealed tube
2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0 - 20 °C / Schlenk technique; Sealed tube
3: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere; Schlenk technique; Sealed tube
With
dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane;
2: |Mitsunobu Displacement / 3: |Sonogashira Cross-Coupling;
DOI:10.1002/anie.201811947