<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>-N-formyl-ethylaminoacetaldehyde diethyl acetal

Base Information

Chemical Name:<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>-N-formyl-ethylaminoacetaldehyde diethyl acetal
CAS No.:84445-10-3
Molecular Formula:C₃₈H₄₅NO₈
Molecular Weight:643.777
Hs Code.:

Synonyms:<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>-N-formyl-ethylaminoacetaldehyde diethyl acetal

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Chemical Property of <α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>-N-formyl-ethylaminoacetaldehyde diethyl acetal

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Technology Process of <α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>-N-formyl-ethylaminoacetaldehyde diethyl acetal

There total 1 articles about <α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>-N-formyl-ethylaminoacetaldehyde diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 64-18-6
formic acid

: 79539-43-8
N-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal oxalate

: 84445-10-3
<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>-N-formyl-ethylaminoacetaldehyde diethyl acetal

Guidance literature:: With sodium formate; acetic anhydride; 1.) 50 deg C, 20 min, 2.) room temp. 1 h;
DOI:10.1248/cpb.30.3197

Reference yield: 100.0%

: 84445-10-3
<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>-N-formyl-ethylaminoacetaldehyde diethyl acetal

: 84423-16-5
5,7-dibenzyloxy-N-formyl-1-(3,4,5-trimethoxybenzyl)-1,2-dihydroisoquinoline

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; for 0.5h; Heating;
DOI:10.1248/cpb.30.3197

Reference yield:

: 84445-10-3
<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>-N-formyl-ethylaminoacetaldehyde diethyl acetal

: 63571-30-2,67950-89-4
(+/-)-TA-073

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / 1 N HCl / tetrahydrofuran / 0.5 h / Heating

2: H₂ / 10percent Pd-C / H₂O; tetrahydrofuran / 22 h / 60 °C / 2427.2 Torr

3: ethanol; aq. H₂SO₄ / 30 h / Heating

With hydrogenchloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; sulfuric acid; water;
DOI:10.1248/cpb.30.3197