4-ethylthio-9,10-dimethoxy-2-mesitylimino-6,7-dihydro-2H-1,3,5-triazino<2,1-a>isoquinoline hydroiodide

Base Information

Chemical Name:4-ethylthio-9,10-dimethoxy-2-mesitylimino-6,7-dihydro-2H-1,3,5-triazino<2,1-a>isoquinoline hydroiodide
CAS No.:85686-92-6
Molecular Formula:C₂₄H₂₈N₄O₂S*HI
Molecular Weight:564.49
Hs Code.:

Synonyms:4-ethylthio-9,10-dimethoxy-2-mesitylimino-6,7-dihydro-2H-1,3,5-triazino<2,1-a>isoquinoline hydroiodide

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Chemical Property of 4-ethylthio-9,10-dimethoxy-2-mesitylimino-6,7-dihydro-2H-1,3,5-triazino<2,1-a>isoquinoline hydroiodide

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Technology Process of 4-ethylthio-9,10-dimethoxy-2-mesitylimino-6,7-dihydro-2H-1,3,5-triazino<2,1-a>isoquinoline hydroiodide

There total 7 articles about 4-ethylthio-9,10-dimethoxy-2-mesitylimino-6,7-dihydro-2H-1,3,5-triazino<2,1-a>isoquinoline hydroiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 85686-89-1
9,10-dimethoxy-2-mesitylamino-6,7-dihydro-4H-1,3,5-triazino<2,1-a>isoquinolin-4-thione

: 75-03-6
ethyl iodide

: 85686-92-6
4-ethylthio-9,10-dimethoxy-2-mesitylimino-6,7-dihydro-2H-1,3,5-triazino<2,1-a>isoquinoline hydroiodide

Guidance literature:: In tetrahydrofuran; for 2h; Heating;

Reference yield:

: 24456-59-5
6,7-dimethoxy-3,4-dihydroisoquinoline-1(2H)-thione

: 85686-92-6
4-ethylthio-9,10-dimethoxy-2-mesitylimino-6,7-dihydro-2H-1,3,5-triazino<2,1-a>isoquinoline hydroiodide

Guidance literature:: Multi-step reaction with 7 steps

2: 80 percent / NH₃ / ethanol / 4 h / Heating

3: 79 percent / sodium hydride / benzene / 16 h / Heating

4: POCl₃ / 2 h / Heating

5: CHCl₃ / 20 h / Heating

6: 80 percent / Lawesson's reagent / dioxane / 16 h / 95 - 100 °C

7: 80 percent / tetrahydrofuran / 2 h / Heating

With Lawessons reagent; ammonia; sodium hydride; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; ethanol; chloroform; benzene;

Reference yield:

: 85686-51-7
9,10-dimethoxy-3,4,6,7-tetrahydro-2H-1,3,5-triazino<2,1-a>isoquinolin-2,4-dione

: 85686-92-6
4-ethylthio-9,10-dimethoxy-2-mesitylimino-6,7-dihydro-2H-1,3,5-triazino<2,1-a>isoquinoline hydroiodide

Guidance literature:: Multi-step reaction with 4 steps

1: POCl₃ / 2 h / Heating

2: CHCl₃ / 20 h / Heating

3: 80 percent / Lawesson's reagent / dioxane / 16 h / 95 - 100 °C

4: 80 percent / tetrahydrofuran / 2 h / Heating

With Lawessons reagent; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; chloroform;