(E)-1-(4-methoxyphenyl)-2-methyl-1-penten-3-one

Base Information

Chemical Name:(E)-1-(4-methoxyphenyl)-2-methyl-1-penten-3-one
CAS No.:75391-06-9
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:

Synonyms:(E)-1-(4-methoxyphenyl)-2-methyl-1-penten-3-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(4-methoxyphenyl)-2-methyl-1-penten-3-one

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Technology Process of (E)-1-(4-methoxyphenyl)-2-methyl-1-penten-3-one

There total 2 articles about (E)-1-(4-methoxyphenyl)-2-methyl-1-penten-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 123-11-5
4-methoxy-benzaldehyde

: 96-22-0
pentan-3-one

: 75391-06-9
(E)-1-(4-methoxyphenyl)-2-methyl-1-penten-3-one

Guidance literature:: With lithium iodide; In diethyl ether; for 72h; Heating;
DOI:10.1039/c39800000486

Reference yield:

: 52750-05-7,119870-81-4,115754-00-2
ethyl (E)-3-(4-methoxyphenyl)-2-methylpropenoate

: 75391-06-9
(E)-1-(4-methoxyphenyl)-2-methyl-1-penten-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: isopropylmagnesium bromide / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2: diethyl ether / 3 h / 0 °C / Inert atmosphere

With isopropylmagnesium bromide; In tetrahydrofuran; diethyl ether;
DOI:10.1039/c6ob00081a

Reference yield: 88.0%

: 924-44-7
glyoxylic acid ethyl ester

: 75391-06-9
(E)-1-(4-methoxyphenyl)-2-methyl-1-penten-3-one

: (E)-thyl 2-hydroxy-6-(4-methoxyphenyl)-3,5-dimethyl-4-oxohex-5-enoate

Guidance literature:: (E)-1-(4-methoxyphenyl)-2-methyl-1-penten-3-one; With n-butyllithium; diisopropylamine; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

glyoxylic acid ethyl ester; In tetrahydrofuran; for 0.333333h;
DOI:10.1039/c6ob00081a