4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside

Base Information

Chemical Name:4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside
CAS No.:1377186-99-6
Molecular Formula:C₅₄H₅₄O₁₁Si
Molecular Weight:907.102
Hs Code.:

Synonyms:4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside

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Technology Process of 4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside

There total 1 articles about 4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 14218-11-2
2,3,4,6-tetra-O-benzoylglucosyl bromide

: 130372-07-5
4-(tret-butyldiphenylsilyloxy)butan-1-ol

: 1377186-99-6
4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside

Guidance literature:: With mercury(I) bromide; mercury(II) cyanide; In 1,2-dichloro-ethane; at 20 ℃; for 36h; Molecular sieve; Inert atmosphere;
DOI:10.1021/ol301105y

Reference yield:

: 1377186-99-6
4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside

: C₂₆H₃₈O₇Si

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 5h; pH=9; Inert atmosphere;
DOI:10.1021/ol301105y

Reference yield:

: 1377186-99-6
4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside

: C₄₅H₅₂O₇Si

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 5 h / 20 °C / pH 9 / Inert atmosphere

2: pyridine; dmap / 6 h / 80 °C / Inert atmosphere

With pyridine; dmap; sodium methylate; In methanol;
DOI:10.1021/ol301105y