4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-Dglucopyranoside

Base Information

Chemical Name:4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-Dglucopyranoside
CAS No.:1377187-00-2
Molecular Formula:C₆₆H₆₄O₁₀Si
Molecular Weight:1045.31
Hs Code.:

Synonyms:4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-Dglucopyranoside

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Chemical Property of 4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-Dglucopyranoside

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Technology Process of 4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-Dglucopyranoside

There total 5 articles about 4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-Dglucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1377186-99-6
4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside

: 1377187-00-2
4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-Dglucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate / methanol / 5 h / 20 °C / pH 9 / Inert atmosphere

2: pyridine; dmap / 6 h / 80 °C / Inert atmosphere

3: pyridine / 10 h / 20 °C

With pyridine; dmap; sodium methylate; In methanol;
DOI:10.1021/ol301105y

Reference yield:

: 14218-11-2
2,3,4,6-tetra-O-benzoylglucosyl bromide

: 1377187-00-2
4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-Dglucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: mercury(I) bromide; mercury(II) cyanide / 1,2-dichloro-ethane / 36 h / 20 °C / Molecular sieve; Inert atmosphere

2: sodium methylate / methanol / 5 h / 20 °C / pH 9 / Inert atmosphere

3: pyridine; dmap / 6 h / 80 °C / Inert atmosphere

4: pyridine / 10 h / 20 °C

With pyridine; dmap; sodium methylate; mercury(I) bromide; mercury(II) cyanide; In methanol; 1,2-dichloro-ethane;
DOI:10.1021/ol301105y

Reference yield:

: 130372-07-5
4-(tret-butyldiphenylsilyloxy)butan-1-ol

: 1377187-00-2
4-tert-butyldiphenylsilyloxybut-1-yl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-β-Dglucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: mercury(I) bromide; mercury(II) cyanide / 1,2-dichloro-ethane / 36 h / 20 °C / Molecular sieve; Inert atmosphere

2: sodium methylate / methanol / 5 h / 20 °C / pH 9 / Inert atmosphere

3: pyridine; dmap / 6 h / 80 °C / Inert atmosphere

4: pyridine / 10 h / 20 °C

With pyridine; dmap; sodium methylate; mercury(I) bromide; mercury(II) cyanide; In methanol; 1,2-dichloro-ethane;
DOI:10.1021/ol301105y