1-((1-(4-methoxyphenyl)vinyl)oxy)-1,1-dimethyl-N,N-bis(trimethylsilyl)silanamine

Base Information

Chemical Name:1-((1-(4-methoxyphenyl)vinyl)oxy)-1,1-dimethyl-N,N-bis(trimethylsilyl)silanamine
CAS No.:1638623-32-1
Molecular Formula:C₁₇H₃₃NO₂Si₃
Molecular Weight:367.711
Hs Code.:

Synonyms:1-((1-(4-methoxyphenyl)vinyl)oxy)-1,1-dimethyl-N,N-bis(trimethylsilyl)silanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-((1-(4-methoxyphenyl)vinyl)oxy)-1,1-dimethyl-N,N-bis(trimethylsilyl)silanamine

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Technology Process of 1-((1-(4-methoxyphenyl)vinyl)oxy)-1,1-dimethyl-N,N-bis(trimethylsilyl)silanamine

There total 3 articles about 1-((1-(4-methoxyphenyl)vinyl)oxy)-1,1-dimethyl-N,N-bis(trimethylsilyl)silanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₁₁H₁₅ClO₂Si

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 1638623-32-1
1-((1-(4-methoxyphenyl)vinyl)oxy)-1,1-dimethyl-N,N-bis(trimethylsilyl)silanamine

Guidance literature:: With triethylamine; In acetonitrile; at 0 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201400405

Reference yield:

: N,N-diethyl-1-((1-(4-methoxyphenyl)vinyl)oxy)-1,1-dimethylsilanamine

: 1638623-32-1
1-((1-(4-methoxyphenyl)vinyl)oxy)-1,1-dimethyl-N,N-bis(trimethylsilyl)silanamine

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere; Schlenk technique

2: triethylamine / acetonitrile / 2 h / 0 °C / Inert atmosphere; Schlenk technique

With triethylamine; acetyl chloride; In tetrahydrofuran; acetonitrile;
DOI:10.1002/anie.201400405

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1638623-32-1
1-((1-(4-methoxyphenyl)vinyl)oxy)-1,1-dimethyl-N,N-bis(trimethylsilyl)silanamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide; triethylamine / acetonitrile / 4 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2: triethylamine / acetonitrile / 2 h / 0 °C / Inert atmosphere; Schlenk technique

With triethylamine; sodium iodide; In acetonitrile;
DOI:10.1002/anie.201400405