Technology Process of C21H13ClO
There total 2 articles about C21H13ClO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; water;
for 11h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium acetate / [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II) / dimethyl sulfoxide / 10 h / 80 °C
2: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 11 h / Reflux
With
potassium acetate; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0); [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II);
In
1,2-dimethoxyethane; water; dimethyl sulfoxide;
1: Miyaura-Ishiyama borylation / 2: Suzuki-Miyaura Coupling;
- Guidance literature:
-
(methoxymethyl)triphenylphosphonium chloride;
With
potassium tert-butylate;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
C21H13ClO;
In
tetrahydrofuran;
at 20 ℃;
for 10h;