4-fluorobenzoic acid 1-carbamoylcyclopropyl ester

Base Information

Chemical Name:4-fluorobenzoic acid 1-carbamoylcyclopropyl ester
CAS No.:1351344-87-0
Molecular Formula:C₁₁H₁₀FNO₃
Molecular Weight:223.204
Hs Code.:

Synonyms:4-fluorobenzoic acid 1-carbamoylcyclopropyl ester

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Chemical Property of 4-fluorobenzoic acid 1-carbamoylcyclopropyl ester

Chemical Property:

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Technology Process of 4-fluorobenzoic acid 1-carbamoylcyclopropyl ester

There total 2 articles about 4-fluorobenzoic acid 1-carbamoylcyclopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1351344-86-9
4-fluorobenzoic acid 1-carboxycyclopropyl ester

: 1351344-87-0
4-fluorobenzoic acid 1-carbamoylcyclopropyl ester

Guidance literature:: 4-fluorobenzoic acid 1-carboxycyclopropyl ester; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; at 20 ℃; for 72h;

With ammonia; In 1,4-dioxane;

Reference yield:

: 403-43-0
4-fluorobenzoyl chloride

: 1351344-87-0
4-fluorobenzoic acid 1-carbamoylcyclopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: chloroform; pyridine / 0.67 h / 70 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / tetrahydrofuran / 72 h / 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; pyridine; chloroform;

Reference yield:

: 1351344-87-0
4-fluorobenzoic acid 1-carbamoylcyclopropyl ester

: 4124-31-6
trichloroacetic acid anhydride

: 1351344-88-1
4-fluorobenzoic acid 1-(5-trichloromethyl[1,2,4]oxadiazol-3-yl)cyclopropyl ester

Guidance literature:: 4-fluorobenzoic acid 1-carbamoylcyclopropyl ester; With triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; at 0 ℃; for 1h;

With water; In tetrahydrofuran;

trichloroacetic acid anhydride; With hydroxylamine; In tetrahydrofuran; ethanol; water; at 60 - 90 ℃; for 4.5h;