ethyl 2,3-dideoxy-(Z)-4-O-propenyl-6-O-trityl-α-D-erythro-hexopyranoside

Base Information

Chemical Name:ethyl 2,3-dideoxy-(Z)-4-O-propenyl-6-O-trityl-α-D-erythro-hexopyranoside
CAS No.:495378-95-5
Molecular Formula:C₃₀H₃₄O₄
Molecular Weight:458.598
Hs Code.:

Synonyms:ethyl 2,3-dideoxy-(Z)-4-O-propenyl-6-O-trityl-α-D-erythro-hexopyranoside

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Chemical Property of ethyl 2,3-dideoxy-(Z)-4-O-propenyl-6-O-trityl-α-D-erythro-hexopyranoside

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Technology Process of ethyl 2,3-dideoxy-(Z)-4-O-propenyl-6-O-trityl-α-D-erythro-hexopyranoside

There total 2 articles about ethyl 2,3-dideoxy-(Z)-4-O-propenyl-6-O-trityl-α-D-erythro-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 495378-94-4
ethyl 4-O-allyl-2,3-dideoxy-6-O-trityl-α-D-erythro-hexopyranoside

: 495378-95-5
ethyl 2,3-dideoxy-(Z)-4-O-propenyl-6-O-trityl-α-D-erythro-hexopyranoside

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; at 50 ℃; for 1.5h;
DOI:10.1016/S0008-6215(02)00139-8

Reference yield:

: 495378-93-3
ethyl 2,3-dideoxy-6-O-trityl-α-D-erythro-hexopyranoside

: 495378-95-5
ethyl 2,3-dideoxy-(Z)-4-O-propenyl-6-O-trityl-α-D-erythro-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / KOH; Bu₄NBr / toluene / 2 h

2: 86 percent / t-BuOK / dimethylsulfoxide / 1.5 h / 50 °C

With potassium hydroxide; potassium tert-butylate; tetrabutylammomium bromide; In dimethyl sulfoxide; toluene;
DOI:10.1016/S0008-6215(02)00139-8

Reference yield: 54.0%

: 1189-71-5
isocyanate de chlorosulfonyle

: 495378-95-5
ethyl 2,3-dideoxy-(Z)-4-O-propenyl-6-O-trityl-α-D-erythro-hexopyranoside

: 495379-09-4
ethyl 2,3-dideoxy-4-O-(3'R,4'S)-(3'-methylazetidin-2'-on-4'-yl)-6-O-trityl-α-D-erythro-hexopyranoside

Guidance literature:: isocyanate de chlorosulfonyle; ethyl 2,3-dideoxy-(Z)-4-O-propenyl-6-O-trityl-α-D-erythro-hexopyranoside; With sodium carbonate; In toluene; at -78 ℃; for 1.5h;

With [(CH₃OC₂H₄O)2AlH₂]Na; In toluene; at -78 ℃; for 0.5h;
DOI:10.1016/S0008-6215(02)00139-8