1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide

Base Information

• Chemical Name: 1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide
• CAS No.: 202208-62-6
• Molecular Formula: C₁₄H₂₅N₄P
• Molecular Weight: 280.353

Synonyms:1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide

Chemical Property of 1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide

Chemical Property:

Purity/Quality:

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Technology Process of 1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide

There total 4 articles about 1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C14H26N4P(1+)*CF3O3S(1-) (1456912-26-7) → 1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide (202208-62-6)

Guidance literature:

With sodium hexamethyldisilazane; In diethyl ether; at -80 - 20 ℃; for 1.75h;

DOI:10.1016/j.tetlet.2013.07.160

Reference yield: 66.0%

1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide (1232774-71-8) → 1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide (202208-62-6)

Guidance literature:

With tris(morpholino)phosphine; In benzene; Inert atmosphere;

DOI:10.1016/j.tet.2010.03.087

Reference yield:

C20H27Br2N4P + dimethyl amine (124-40-3) → 1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide (202208-62-6)

Guidance literature:

With triethylamine; In dichloromethane; at 10 - 20 ℃; for 0.333333h;

DOI:10.1002/hc.21283

upstream raw materials:

1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide

C₁₄H₂₆N₄P⁽¹⁺⁾*CF₃O₃S^(1-)

N,N-dimethyl-N'-p-tolylformimidamide

dimethyl amine

Downstream raw materials:

1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide

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