1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide

Base Information

Chemical Name:1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide
CAS No.:1232774-71-8
Molecular Formula:C₁₄H₂₅N₄PSe
Molecular Weight:359.313
Hs Code.:

Synonyms:1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide

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Chemical Property of 1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide

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Technology Process of 1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide

There total 4 articles about 1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1232774-52-5
N,N-dimethyl-N'-(4-methylphenyl)-P-(trichloromethyl)-phosphonoselenoic diamide

: 124-40-3
dimethyl amine

: 1232774-71-8
1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide

Guidance literature:: at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1016/j.tet.2010.03.087

Reference yield:

: 202208-62-6
1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide

: 1232774-71-8
1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide

Guidance literature:: With selenium; In dichloromethane; for 0.166667h;
DOI:10.1002/hc.21283

Reference yield:

: C₂₀H₂₇Br₂N₄P

: 1232774-71-8
1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0.33 h / 10 - 20 °C

2: selenium / dichloromethane / 0.17 h

With selenium; triethylamine; In dichloromethane;
DOI:10.1002/hc.21283