C₁₁H₈BrFN₂O

Base Information

Chemical Name:C₁₁H₈BrFN₂O
CAS No.:1514914-92-1
Molecular Formula:C₁₁H₈BrFN₂O
Molecular Weight:283.1
Hs Code.:

C<sub>11</sub>H<sub>8</sub>BrFN<sub>2</sub>O

Synonyms:C₁₁H₈BrFN₂O

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Chemical Property of C₁₁H₈BrFN₂O

Chemical Property:

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Technology Process of C₁₁H₈BrFN₂O

There total 8 articles about C₁₁H₈BrFN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39856-50-3
5-bromo2-nitropyridine

: 62257-16-3
5-hydroxy-2-fluoroaniline

: 1020173-38-9
2-fluoro-5-(6-nitropyridin-3-yloxy)benzenamine

: 1514914-92-1
C₁₁H₈BrFN₂O

Guidance literature:: With potassium phosphate; In water; dimethyl sulfoxide; at 70 - 75 ℃; for 10h; Reagent/catalyst; Solvent;
DOI:10.1021/op4002824

Reference yield:

: 84478-75-1
2-chloro-4-fluoro-5-nitrophenol

: 1514914-92-1
C₁₁H₈BrFN₂O

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate; palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C

2: potassium phosphate / water; dimethyl sulfoxide / 10 h / 70 - 75 °C

With potassium phosphate; palladium 10% on activated carbon; hydrogen; sodium acetate; In methanol; water; dimethyl sulfoxide;
DOI:10.1021/op4002824

Reference yield:

: 1996-41-4
2-chloro-4-fluorophenol

: 1514914-92-1
C₁₁H₈BrFN₂O

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / water / 1 h / 40 - 45 °C / Large scale

1.2: 1 h / 10 - 25 °C / Large scale

2.1: sulfuric acid; nitric acid / 1 h / 0 - 15 °C / Large scale

3.1: methanol; sodium hydroxide / 1.67 h / 20 - 40 °C / Large scale

4.1: sodium acetate; palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C

5.1: potassium phosphate / water; dimethyl sulfoxide / 10 h / 70 - 75 °C

With methanol; potassium phosphate; sulfuric acid; palladium 10% on activated carbon; hydrogen; nitric acid; sodium acetate; sodium carbonate; sodium hydroxide; In methanol; water; dimethyl sulfoxide;
DOI:10.1021/op4002824