4-methylphenyl 2,3-O-1-methylethylidene-1-thio-β-D-ribopentodialdo-1,4-furanoside

Base Information

Chemical Name:4-methylphenyl 2,3-O-1-methylethylidene-1-thio-β-D-ribopentodialdo-1,4-furanoside
CAS No.:1356826-94-2
Molecular Formula:C₁₅H₁₈O₄S
Molecular Weight:294.372
Hs Code.:

Synonyms:4-methylphenyl 2,3-O-1-methylethylidene-1-thio-β-D-ribopentodialdo-1,4-furanoside

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Chemical Property of 4-methylphenyl 2,3-O-1-methylethylidene-1-thio-β-D-ribopentodialdo-1,4-furanoside

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Technology Process of 4-methylphenyl 2,3-O-1-methylethylidene-1-thio-β-D-ribopentodialdo-1,4-furanoside

There total 2 articles about 4-methylphenyl 2,3-O-1-methylethylidene-1-thio-β-D-ribopentodialdo-1,4-furanoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₁₅H₂₀O₄S

: 1356826-94-2
4-methylphenyl 2,3-O-1-methylethylidene-1-thio-β-D-ribopentodialdo-1,4-furanoside

Guidance literature:: With magnesium sulfate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 8h;

Reference yield:

: 1131610-84-8
p-tolyl 1-thio-β-D-ribofuranoside

: 1356826-94-2
4-methylphenyl 2,3-O-1-methylethylidene-1-thio-β-D-ribopentodialdo-1,4-furanoside

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium sulfate / (1S)-10-camphorsulfonic acid / acetone / 5 h / 20 °C

2: magnesium sulfate; Dess-Martin periodane / dichloromethane / 8 h / 20 °C

With magnesium sulfate; Dess-Martin periodane; (1S)-10-camphorsulfonic acid; In dichloromethane; acetone;

Reference yield:

: 1356826-94-2
4-methylphenyl 2,3-O-1-methylethylidene-1-thio-β-D-ribopentodialdo-1,4-furanoside

: 75-16-1
methylmagnesium bromide

: 1356826-96-4
4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-α-L-allofuranoside

: 1356826-95-3
4-methylphenyl 6-deoxy-2,3-O-1-methylethylidene-1-thio-β-Dallofuranoside

Guidance literature:: 4-methylphenyl 2,3-O-1-methylethylidene-1-thio-β-D-ribopentodialdo-1,4-furanoside; methylmagnesium bromide; In tetrahydrofuran; at -30 ℃; for 2.5h;

With ammonium chloride; In tetrahydrofuran; water;