(S)-benzyl(2-((1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxopropan-2-yl)amino)-2-oxoethyl)carmabamate

Base Information

Chemical Name:(S)-benzyl(2-((1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxopropan-2-yl)amino)-2-oxoethyl)carmabamate
CAS No.:1381763-25-2
Molecular Formula:C₁₉H₁₉N₅O₄
Molecular Weight:381.391
Hs Code.:

Synonyms:(S)-benzyl(2-((1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxopropan-2-yl)amino)-2-oxoethyl)carmabamate

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Chemical Property of (S)-benzyl(2-((1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxopropan-2-yl)amino)-2-oxoethyl)carmabamate

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Technology Process of (S)-benzyl(2-((1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxopropan-2-yl)amino)-2-oxoethyl)carmabamate

There total 3 articles about (S)-benzyl(2-((1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxopropan-2-yl)amino)-2-oxoethyl)carmabamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 3079-63-8
(S)-2-(2-Benzyloxycarbonylamino-acetylamino)-propionic acid

: 1381763-25-2
(S)-benzyl(2-((1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxopropan-2-yl)amino)-2-oxoethyl)carmabamate

Guidance literature:: With thionyl chloride; In dichloromethane; at -15 - 20 ℃; for 6.5h; Inert atmosphere;
DOI:10.1016/j.bmc.2013.12.017

Reference yield:

: 173459-80-8
benzyl [2?(1H?benzo[d][1,2,3]triazol?1?yl)?2?oxoethyl]carbamate

: 1381763-25-2
(S)-benzyl(2-((1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxopropan-2-yl)amino)-2-oxoethyl)carmabamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / acetonitrile; water / 16 h

2: thionyl chloride / dichloromethane / 6.5 h / -15 - 20 °C / Inert atmosphere

With thionyl chloride; triethylamine; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmc.2013.12.017

Reference yield:

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 1381763-25-2
(S)-benzyl(2-((1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxopropan-2-yl)amino)-2-oxoethyl)carmabamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / tetrahydrofuran / 0.33 h / 20 °C

1.2: 2 h / 20 °C

2.1: triethylamine / acetonitrile; water / 16 h

3.1: thionyl chloride / dichloromethane / 6.5 h / -15 - 20 °C / Inert atmosphere

With thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmc.2013.12.017