3-cyclopentyl-2-{4-[(pyridine-3-carbonyl)-amino]-phenyl}-propionic acid

Base Information

• Chemical Name: 3-cyclopentyl-2-{4-[(pyridine-3-carbonyl)-amino]-phenyl}-propionic acid
• CAS No.: 372938-21-1
• Molecular Formula: C₂₀H₂₂N₂O₃
• Molecular Weight: 338.406

Synonyms:3-cyclopentyl-2-{4-[(pyridine-3-carbonyl)-amino]-phenyl}-propionic acid

Chemical Property of 3-cyclopentyl-2-{4-[(pyridine-3-carbonyl)-amino]-phenyl}-propionic acid

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Technology Process of 3-cyclopentyl-2-{4-[(pyridine-3-carbonyl)-amino]-phenyl}-propionic acid

There total 1 articles about 3-cyclopentyl-2-{4-[(pyridine-3-carbonyl)-amino]-phenyl}-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.7%

2-(4-amino-phenyl)-3-cyclopentyl-propionic acid (372938-18-6) + pyridine-3-carbonyl chloride hydrochloride (20260-53-1) → 3-cyclopentyl-2-{4-[(pyridine-3-carbonyl)-amino]-phenyl}-propionic acid (372938-21-1)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

Reference yield: 39.5%

3-cyclopentyl-2-{4-[(pyridine-3-carbonyl)-amino]-phenyl}-propionic acid (372938-21-1) + ethyl 2-amino-1,3-thiazol-4-acetate (53266-94-7) + (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate (56602-33-6) → [2-(3-cyclopentyl-2-{4-[(pyridine-3-carbonyl)-amino]-phenyl}-propionylamino)-thiazol-4-yl]-acetic acid ethyl ester

Guidance literature:

With triethylamine; In dichloromethane; ethyl acetate;

Reference yield: 12.5%

2-aminothiazole-4-carboxylate (5398-36-7) + 3-cyclopentyl-2-{4-[(pyridine-3-carbonyl)-amino]-phenyl}-propionic acid (372938-21-1) + oxalyl dichloride (79-37-8) → 2-(3-Cyclopentyl-2-{4-[(pyridine-3-carbonyl)-amino]-phenyl}propionylamino)-thiazole-4-carboxylic acid ethyl ester (372938-10-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;

upstream raw materials:

2-(4-amino-phenyl)-3-cyclopentyl-propionic acid

pyridine-3-carbonyl chloride hydrochloride

Downstream raw materials:

2-(3-Cyclopentyl-2-{4-[(pyridine-3-carbonyl)-amino]-phenyl}propionylamino)-thiazole-4-carboxylic acid ethyl ester

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