p-toluyl 2-O-benzoyl-4,6-O-benzylidene-3-O-fluorenylmethoxycarbonyl-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:p-toluyl 2-O-benzoyl-4,6-O-benzylidene-3-O-fluorenylmethoxycarbonyl-1-thio-β-D-galactopyranoside
CAS No.:1260145-65-0
Molecular Formula:C₄₂H₃₆O₈S
Molecular Weight:700.809
Hs Code.:

Synonyms:p-toluyl 2-O-benzoyl-4,6-O-benzylidene-3-O-fluorenylmethoxycarbonyl-1-thio-β-D-galactopyranoside

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Chemical Property of p-toluyl 2-O-benzoyl-4,6-O-benzylidene-3-O-fluorenylmethoxycarbonyl-1-thio-β-D-galactopyranoside

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Technology Process of p-toluyl 2-O-benzoyl-4,6-O-benzylidene-3-O-fluorenylmethoxycarbonyl-1-thio-β-D-galactopyranoside

There total 3 articles about p-toluyl 2-O-benzoyl-4,6-O-benzylidene-3-O-fluorenylmethoxycarbonyl-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1260145-66-1
C₃₅H₃₂O₇S

: 98-88-4
benzoyl chloride

: 1260145-65-0
p-toluyl 2-O-benzoyl-4,6-O-benzylidene-3-O-fluorenylmethoxycarbonyl-1-thio-β-D-galactopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 0 - 23 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja1087375

Reference yield:

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1260145-65-0
p-toluyl 2-O-benzoyl-4,6-O-benzylidene-3-O-fluorenylmethoxycarbonyl-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

2: pyridine / dichloromethane / 1 h / 0 - 23 °C / Inert atmosphere

With pyridine; In dichloromethane;
DOI:10.1021/ja1087375

Reference yield:

: 220645-86-3
p-methylphenyl 4,6-O-benzylidene-1-thio-β-D-galactopyranoside

: 1260145-65-0
p-toluyl 2-O-benzoyl-4,6-O-benzylidene-3-O-fluorenylmethoxycarbonyl-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

2: pyridine / dichloromethane / 1 h / 0 - 23 °C / Inert atmosphere

With pyridine; In dichloromethane;
DOI:10.1021/ja1087375