3-(2-{5-[3,4-Dimethyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-3,4-dimethyl-1H-pyrrole-2-carbonyl}-phenyl)-propionic acid methyl ester

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Chemical Name:3-(2-{5-[3,4-Dimethyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-3,4-dimethyl-1H-pyrrole-2-carbonyl}-phenyl)-propionic acid methyl ester
CAS No.:204994-94-5
Molecular Formula:C₂₄H₂₆N₂O₄
Molecular Weight:406.481
Hs Code.:

Synonyms:3-(2-{5-[3,4-Dimethyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-3,4-dimethyl-1H-pyrrole-2-carbonyl}-phenyl)-propionic acid methyl ester

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Chemical Property of 3-(2-{5-[3,4-Dimethyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-3,4-dimethyl-1H-pyrrole-2-carbonyl}-phenyl)-propionic acid methyl ester

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Technology Process of 3-(2-{5-[3,4-Dimethyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-3,4-dimethyl-1H-pyrrole-2-carbonyl}-phenyl)-propionic acid methyl ester

There total 4 articles about 3-(2-{5-[3,4-Dimethyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-3,4-dimethyl-1H-pyrrole-2-carbonyl}-phenyl)-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33779-03-2
2-(2-methoxycarbonylethyl)benzoic acid

: 204994-94-5
3-(2-{5-[3,4-Dimethyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-3,4-dimethyl-1H-pyrrole-2-carbonyl}-phenyl)-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / thionyl chloride / 0.17 h / 50 °C

2: 95 percent / tin tetrachloride / CH₂Cl₂ / 1.) 0 deg C, 20 min, 2.) room temperature, 2 h

With thionyl chloride; tin(IV) chloride; In dichloromethane;
DOI:10.1021/jo972227r

Reference yield:

: 776-79-4
2-(2-carboxyethyl)benzoic acid

: 204994-94-5
3-(2-{5-[3,4-Dimethyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-3,4-dimethyl-1H-pyrrole-2-carbonyl}-phenyl)-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 0.5 h / Ambient temperature

2: 66 percent / thionyl chloride / 0.17 h / 50 °C

3: 95 percent / tin tetrachloride / CH₂Cl₂ / 1.) 0 deg C, 20 min, 2.) room temperature, 2 h

With thionyl chloride; sulfuric acid; tin(IV) chloride; In dichloromethane;
DOI:10.1021/jo972227r

Reference yield:

: 18454-53-0
(E)-o-carboxycinnamic acid

: 204994-94-5
3-(2-{5-[3,4-Dimethyl-5-oxo-1,5-dihydro-pyrrol-(2Z)-ylidenemethyl]-3,4-dimethyl-1H-pyrrole-2-carbonyl}-phenyl)-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / Raney nickel, NaOH / H₂O

2: sulfuric acid / 0.5 h / Ambient temperature

3: 66 percent / thionyl chloride / 0.17 h / 50 °C

4: 95 percent / tin tetrachloride / CH₂Cl₂ / 1.) 0 deg C, 20 min, 2.) room temperature, 2 h

With sodium hydroxide; thionyl chloride; sulfuric acid; tin(IV) chloride; nickel; In dichloromethane; water;
DOI:10.1021/jo972227r